Synthesis of new C60-donor dyads by reaction of pyrazolylhydrazones with [60]fullerene under microwave irradiation

被引：49

作者：

de la Cruz, P

Díaz-Ortiz, A

García, JJ

Gómez-Escalonilla, MJ

de la Hoz, A

Langa, F

机构：

[1] Univ Castilla La Mancha, Fac Ciencias Medio Ambiente, Dept Q Organ, E-45001 Toledo, Spain

[2] Univ Castilla La Mancha, Fac Quim, Dept Quim Organ, E-13071 Ciudad Real, Spain

来源：

TETRAHEDRON LETTERS | 1999年 / 40卷 / 08期

关键词：

D O I：

10.1016/S0040-4039(98)02651-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A facile synthesis of a series of pyrazolo[4,5'][60]fullerenes from pyrazolyl hydrazones under microwave irradiation is described. Evidence of intramolecular charge transfer internation is shown. (C) 1999 Elsevier Science Ltd. All rights reserved.

引用

页码：1587 / 1590

页数：4

共 16 条

[1] Electron transfer from tetrathiafulvalenes to photoexcited C-70 studied by observing transient absorption in the near-IR region [J].

Alam, MM ;

Watanabe, A ;

Ito, O .

BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1997, 70 (08) :1833-1838

[2] Efficient photoinduced electron transfer between C-60 and tetrathiafulvalenes studied by nanosecond laser photolysis [J].

Alam, MM ;

Watanabe, A ;

Ito, O .

JOURNAL OF PHOTOCHEMISTRY AND PHOTOBIOLOGY A-CHEMISTRY, 1997, 104 (1-3) :59-64

[3] Efficient tautomerization hydrazone-azomethine imine under microwave irradiation.: Synthesis of [4,3′] and [5,3′]bipyrazoles [J].

Arrieta, A ;

Carrillo, JR ;

Cossío, FP ;

Díaz-Ortiz, A ;

Gómez-Escalonilla, MJ ;

de la Hoz, A ;

Langa, F ;

Moreno, A .

TETRAHEDRON, 1998, 54 (43) :13167-13180

[4] PREPARATION AND CHARACTERIZATION OF C-60(FERROCENE)2 [J].

CRANE, JD ;

HITCHCOCK, PB ;

KROTO, HW ;

TAYLOR, R ;

WALTON, DRM .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1992, (24) :1764-1765

[5] Stereocontrolled total synthesis of (+)-paraherquamide B [J].

Cushing, TD ;

SanzCervera, JF ;

Williams, RM .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (03) :557-579

[6]

Diekers M, 1998, EUR J ORG CHEM, V1998, P1111, DOI 10.1002/(SICI)1099-0690(199806)1998:6<1111::AID-EJOC1111>3.0.CO

[7]

2-B

[8]

FINAR IL, 1957, J CHEM SOC, P3314

[9] AN X-RAY CRYSTALLOGRAPHIC ANALYSIS OF A (BEDT-TTF)2C60 CHARGE-TRANSFER COMPLEX [J].

IZUOKA, A ;

TACHIKAWA, T ;

SUGAWARA, T ;

SUZUKI, Y ;

KONNO, M ;

SAITO, Y ;

SHINOHARA, H .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1992, (19) :1472-1473

[10]

Langa F., UNPUB

← 1 2 →