Synthesis and characterization of CdIn2S4 nanorods by converting CdS nanorods via the hydrothermal route

被引：47

作者：

Hu, JQ

Deng, B

Zhang, WX

Tang, KB

Qian, YT

机构：

[1] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China

[2] Univ Sci & Technol China, Struct Res Lab, Anhua 230026, Peoples R China

来源：

INORGANIC CHEMISTRY | 2001年 / 40卷 / 13期

关键词：

D O I：

10.1021/ic001202z

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The ternary semiconductor CdIn2S4 nanorods were synthesized by a method based on CdS nanorods via the hydrothermal route, in which CdS nanorods were converted by reaction with InCl3 and thiourea in aqueous-solution Transmission electronmicroscopy (TEM) images revealed that the typical sizes of the CdIn2S4 nanorods were 10-30 nm in diameter and 200-1000 nm in length. X-ray photoelectron spectra (XPS) analysis of the surface stoichiometry (CdIn2.03S4.15) and room-temperature Raman spectrum (RS) were recorded. The influences of reaction temperature, time, and sulfur sources on the formation for CdIn2S4 nanorods were investigated. A possible formation mechanism of the CdIn2S4 nanorods was also proposed.

引用

页码：3130 / 3133

页数：4

共 40 条

[1] A systematic FT-Raman spectroscopic study of twelve bis-thiourea complexes, A(tu)2B2 (A = Zn, Cd, Hg; B=Cl, Br, I, SCN) [J].