Synthesis of molybdenum (IV) disulfide using a single-source method

被引:11
作者
Monteiro, OC [1 ]
Trindade, T [1 ]
机构
[1] Univ Aveiro, Dept Chem, CICECO, P-3810193 Aveiro, Portugal
关键词
metal sulfides; chemical synthesis; microstructure;
D O I
10.1016/j.materresbull.2003.11.001
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Molybdenum(IV) disulfide was prepared by the thermalysis of the single molecule precursor [Mo2O4(S2C- NEt2)(2)] (Et: ethyl group). The thermalysis was monitored by thermogravimetric analysis and FT-infrared spectroscopy. The MoS2 materials obtained during the thermalysis experiments were characterized in terms of their morphological and optical characteristics. (C) 2003 Elsevier Ltd. All rights reserved.
引用
收藏
页码:357 / 363
页数:7
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