Hybrid silica gel polytetrahydrofuran thin films

被引：6

作者：

Fidalgo, A ^{[1
]}

Ilharco, L ^{[1
]}

机构：

[1] Univ Tecn Lisboa, Ctr Quim Fis Mol, Inst Super Tecn, P-1096 Lisbon, Portugal

来源：

JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY | 1998年 / 13卷 / 1-3期

关键词：

hybrid films; polytetrahydrofuran; FTIR; SEM;

D O I：

10.1023/A:1008625328672

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

The sol-gel process has been used to prepare hybrid silica gel-polytetrahydrofuran (PTHF) thin films, using tetraethylorthosilicate (TEOS) as the precursor. The films were prepared by spin-coating, and characterized by profilometry, transmission FTIR and SEM. Film properties were conditioned by the preparation procedure as well as by the initial recipe, namely the solvent, polymer content and molecular weight. Evidence was obtained of the participation of the polymer in the condensation step of the process, interacting by hydrogen bonds with hydroxyl groups of the silicate network.

引用

页码：433 / 437

页数：5