Dynamic mechanical and morphological properties of polycarbonate/multi-walled carbon nanotube composites

被引:89
作者
Sung, YT
Kum, CK
Lee, HS
Byon, NS
Yoon, HG
Kim, WN [1 ]
机构
[1] Korea Univ, Dept Chem & Biol Engn, Appl Rheol Ctr, Seoul 136701, South Korea
[2] LG Chem Ltd, Tech Ctr, Taejon 305343, South Korea
[3] Korea Univ, Dept Mat Sci, Seoul 136701, South Korea
基金
欧洲研究理事会;
关键词
multi-walled carbon nanotube; composite; dynamic mechanical properties;
D O I
10.1016/j.polymer.2005.04.075
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
Dynamic mechanical and morphological properties of the polycarbonate (PC)/multi-walled carbon nanotube (MWNT) composites were studied by dynamic mechanical thermal analysis (DMTA) and X-ray diffractometry, respectively. For the without annealed PC/MWNT composites containing the higher content of the MWNT (>= 7.0 wt%), double tan delta peaks were observed, which could be explained by the phase separation morphology model. For the annealed PC/MWNT composites, a broad single tan 5 peak was observed. From the X-ray diffraction of the annealed PC/MWNT composites, it was observed that more regular structure of the PC was obtained, which was consistent with the result of the thermal analysis of the annealed PC/MWNT composites. From the dynamic mechanical properties, thermal analysis, and X-ray diffraction of the annealed PC/MWNT composites, it is suggested that PC/MWNT composites show a broad single tan delta peak and partially crystalline structure of the PC in the PC/MWNT composites by annealing. (c) 2005 Elsevier Ltd. All rights reserved.
引用
收藏
页码:5656 / 5661
页数:6
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