Preparation of Cd1-xZnxSe using microwave-assisted polyol synthesis

被引:43
作者
Grisaru, H
Palchik, O
Gedanken, A [1 ]
Palchik, V
Slifkin, MA
Weiss, AN
Hacohen, YR
机构
[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel
[2] Jerusalem Coll Technol, Dept Elect, IL-91160 Jerusalem, Israel
[3] Weizmann Inst Sci, Dept Mat & Interfaces, IL-76100 Rehovot, Israel
基金
加拿大健康研究院;
关键词
D O I
10.1021/ic0155479
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A new method for the preparation of a nanophased ternary selenide is described. The synthesis employs microwave heating for the preparation of Cd1-xZnxSe. The reaction was carried out in basic ethylene glycol, which serves both as a solvent and reducing agent. The resulting compound was composed of monodispersed nanoparticles with an average diameter of 6 nm. The particles were characterized using TEM, HR-TEM, XRD, and photoacoustic spectroscopy (PAS). (CH3COO)(2)Cd.2H(2)O + (CH3COO)(2),Zn.2H(2)O + Se --> (Microwave) CdZnSe.
引用
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页码:4814 / +
页数:3
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