Preparation of Cd1-xZnxSe using microwave-assisted polyol synthesis

被引：43

作者：

Grisaru, H

Palchik, O

Gedanken, A ^{[1
]}

Palchik, V

Slifkin, MA

Weiss, AN

Hacohen, YR

机构：

[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel

[2] Jerusalem Coll Technol, Dept Elect, IL-91160 Jerusalem, Israel

[3] Weizmann Inst Sci, Dept Mat & Interfaces, IL-76100 Rehovot, Israel

来源：

INORGANIC CHEMISTRY | 2001年 / 40卷 / 19期

基金：

加拿大健康研究院;

关键词：

D O I：

10.1021/ic0155479

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new method for the preparation of a nanophased ternary selenide is described. The synthesis employs microwave heating for the preparation of Cd1-xZnxSe. The reaction was carried out in basic ethylene glycol, which serves both as a solvent and reducing agent. The resulting compound was composed of monodispersed nanoparticles with an average diameter of 6 nm. The particles were characterized using TEM, HR-TEM, XRD, and photoacoustic spectroscopy (PAS). (CH3COO)(2)Cd.2H(2)O + (CH3COO)(2),Zn.2H(2)O + Se --> (Microwave) CdZnSe.

引用

页码：4814 / +

页数：3

共 27 条

[21] SHARMA KC, 1988, INDIAN J PURE AP PHY, V26, P480
[22] SLIFKIN MA, 1998, SPIE INT SOC OPT ENG, V3110, P481
[23] EMS - A SOFTWARE PACKAGE FOR ELECTRON-DIFFRACTION ANALYSIS AND HREM IMAGE SIMULATION IN MATERIALS SCIENCE
STADELMANN, PA
[J]. ULTRAMICROSCOPY, 1987, 21 (02) : 131 - 145
[24] Wang WH, 1998, ADV MATER, V10, P1479, DOI 10.1002/(SICI)1521-4095(199812)10:17<1479::AID-ADMA1479>3.0.CO
[25] 2-M
[26] Preparation and characterization of nanocrystalline Cu2-xSe by a novel solvothermal pathway
Wang, WZ
Yan, P
Liu, FY
Xie, Y
Geng, Y
Qian, YT
[J]. JOURNAL OF MATERIALS CHEMISTRY, 1998, 8 (11) : 2321 - 2322
[27] Microwave assisted preparation of CdSe, PbSe, and Cu2-xSe nanoparticles
Zhu, JJ
Palchik, O
Chen, SG
Gedanken, A
[J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (31) : 7344 - 7347

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