Synthesis of flower- and rod-like nickel sulfide nanostructures by an organic-free hydrothermal process

被引：35

作者：

Pan, Qingtao ^{[1
]}

Huang, Kai ^{[1
]}

Ni, Shibing ^{[1
]}

Yang, Feng ^{[1
]}

He, Deyan ^{[1
]}

机构：

[1] Lanzhou Univ, Dept Phys, Lanzhou 730000, Peoples R China

来源：

MATERIALS RESEARCH BULLETIN | 2008年 / 43卷 / 06期

关键词：

inorganic compounds; nanostructures; chemical synthesis; optical properties;

D O I：

10.1016/j.materresbull.2007.06.038

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Well-crystalline flower- and rod-like NiS nanostructures have been synthesized by an organic-free hydrothermal process at a low temperature of 200 degrees C. X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM) were employed to characterize the as-synthesized NiS nanostructures. The effects of temperature and reaction time on the morphology have been also investigated. The two-step flake-cracking mechanism for the formation of flower- and rodlike NiS nanostructures was discussed. The products were also investigated by photoluminescence (PL) spectroscopy. (C) 2007 Elsevier Ltd. All rights reserved.

引用

页码：1440 / 1447

页数：8

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