A simple, rapid and efficient protocol for the selective phosphorylation of phenols with dibenzyl phosphite

被引：74

作者：

Silverberg, LJ

Dillon, JL

Vemishetti, P

机构：

[1] Bristol-Myers Squibb Company, Process Exploration Labs., Syracuse, NY 13221-4755

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 06期

关键词：

D O I：

10.1016/0040-4039(95)02294-5

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Phosphorylation of phenols with dibenzyl phosphite, carbon tetrachloride, N,N-diisopropylethylamine, and catalytic DMAP in acetonitrile at -10 degrees C is rapid, mild, clean, high yielding, and selective.

引用

页码：771 / 774

页数：4

共 28 条

[1] STUDIES ON PHOSPHORYLATION .3. FURTHER OBSERVATIONS ON THE REACTION OF PHOSPHITES WITH POLYHALOGEN COMPOUNDS IN PRESENCE OF BASES AND ITS APPLICATION TO THE PHOSPHORYLATION OF ALCOHOLS
ATHERTON, FR
TODD, AR
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1947, (MAY): : 674 - 678
[2] STUDIES ON PHOSPHORYLATION .2. THE REACTION OF DIALKYL PHOSPHITES WITH POLYHALOGEN COMPOUNDS IN PRESENCE OF BASES - A NEW METHOD FOR THE PHOSPHORYLATION OF AMINES
ATHERTON, FR
OPENSHAW, HT
TODD, AR
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1945, (SEP-): : 660 - 663
[3] STUDIES ON PHOSPHORYLATION .1. DIBENZYL CHLOROPHOSPHONATE AS A PHOSPHORYLATING AGENT
ATHERTON, FR
OPENSHAW, HT
TODD, AR
[J]. JOURNAL OF THE CHEMICAL SOCIETY, 1945, (MAY): : 382 - 385
[4] CHEMOSELECTIVE DEPROTECTION OF BENZYL-ESTERS IN THE PRESENCE OF BENZYL ETHERS, BENZYLOXYMETHYL ETHERS AND N-BENZYL GROUPS BY CATALYTIC TRANSFER HYDROGENATION
BAJWA, JS
[J]. TETRAHEDRON LETTERS, 1992, 33 (17) : 2299 - 2302
[5] BATRA BS, 1991, INDIAN J CHEM B, V30, P57
[6] BATRA BS, 1989, TETRAHEDRON LETT, V30, P1687
[7] FAVREAU D, Patent No. 53755
[8] FIESER LF, 1967, REAGENTS ORGANIC SYN, V1, P198
[9] FRIEDMAN OM, 1954, J AM CHEM SOC, P916
[10] 4-DIALKYLAMINOPYRIDINES AS ACYLATION CATALYSTS .4. 4-DIALKYLAMINOPYRIDINES AS HIGHLY ACTIVE ACYLATION CATALYSTS
HOFLE, G
STEGLICH, W
VORBRUGGEN, H
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1978, 17 (08): : 569 - &

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