Identification of volatile organic compounds emitted by a naturally aged book using solid-phase microextraction/gas chromatography/mass spectrometry

被引：84

作者：

Lattuati-Derieux, A ^{[1
]}

Bonnassies-Termes, S ^{[1
]}

Lavédrine, B ^{[1
]}

机构：

[1] Museum Natl Hist Nat, CNRS, MCC, MNHN,CRCDG,FRE 2743, F-75231 Paris 05, France

来源：

JOURNAL OF CHROMATOGRAPHY A | 2004年 / 1026卷 / 1-2期

关键词：

paper; cellulose; ageing; solid-phase microextraction; headspace analysis; volatile organic compounds;

D O I：

10.1016/j.chroma.2003.11.069

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Solid-phase microextraction (SPME) coupled to gas chromatography/mass spectrometry (GC/MS) has been applied to the analysis of volatile organic compounds emitted from a naturally aged groundwood pulp paper originating from an old book in order to access the products produced through the decomposition reactions occurring in paper upon ageing. Two different extraction methods were developed and compared: headspace SPME and contact SPME. The influence of few extraction parameters were tested in order to define the best extraction conditions. An optimised non-destructive contact SPME method was elaborated and allowed the characterisation of more than 50 individual constituents. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：9 / 18

页数：10

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