Preparation of La(Zn0.5Ti0.5)O3 powders via citric acid precursor

被引：13

作者：

Cao, W

Xu, YB ^{[1
]}

Wang, SJ

Lu, PX

Huang, GH

Xu, CF

机构：

[1] Huazhong Univ Sci & Technol, State Key Lab Laser Technol, Wuhan 430074, Peoples R China

[2] Guangxi Teachers Coll, Dept Phys, Nanning 530001, Peoples R China

[3] Huazhong Univ Sci & Technol, State Key Lab Coal Combust, Wuhan 430074, Peoples R China

来源：

MATERIALS LETTERS | 2005年 / 59卷 / 14-15期

关键词：

chemical synthesis; citric acid; La(Zn0.5Ti0.5)O-3;

D O I：

10.1016/j.matlet.2005.02.025

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

La(Zn0.5Ti0.5)O-3 powders were synthesized by the Pechini process using citric acid as a complexing agent. The effect of the molar ratio of citric acid to total metal cations concentration (CA/M) and the pH of the starting solution on the crystallization behavior of La(Zn0.5Ti0.5)O-3 was investigated. Homogeneously mixed gel was obtained and transferred into resin through charring. Single-phase and well-crystallized La(Zn0.5Ti0.5)O-3 powders were obtained at 1000 degrees C for 2 h. DSC, TG and XRD were used to characterize the precursors and derived powders. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：1914 / 1918

页数：5

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