Synthesis and characterization of MCM-41-type composite materials prepared from ZSM-5 zeolite
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作者:
Song, Chun-Min
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China Univ Petr, CNPC, Key Lab Catalysis, State Key Lab Heavy Oil Proc, Dongying 257061, Peoples R ChinaChina Univ Petr, CNPC, Key Lab Catalysis, State Key Lab Heavy Oil Proc, Dongying 257061, Peoples R China
Song, Chun-Min
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机构:
Jiang, Jie
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机构:
Yan, Zi-feng
[1
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机构:
[1] China Univ Petr, CNPC, Key Lab Catalysis, State Key Lab Heavy Oil Proc, Dongying 257061, Peoples R China
Micro/mesoporous composite materials with microporous and mesoporous double pores-size distribution were hydrothermally synthesized by using slurry or filtrate of alkali-treated ZSM-5 zeolite and were characterized by XRD, N-2 adsorption, FT-IR, TEM and so on. The XRD and TEM patterns indicate the composite materials possess ordered hexagonal structure. The sample MZ-B using filtrate of alkali-treated ZSM-5 zeolite hardly contains raw ZSM-5 particles. However, sample MZ-A originated from the slurry of alkali-treated ZSM-5 zeolite may contain some ZSM-5 crystallites, owing to the differences in concentration and time of alkaline treatment for ZSM-5 zeolite.