(R)-(+)-2.2′-diamino-1,1′-binaphthyl

被引:12
作者
Jones, MD [1 ]
Paz, FAA [1 ]
Davies, JE [1 ]
Johnson, BFG [1 ]
机构
[1] Univ Cambridge, Dept Chem, Cambridge CB2 1EW, England
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷
关键词
D O I
10.1107/S1600536803011681
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the title compound, C20H16N2, has been determined at 180 (2) K in the chiral space group P4(3)2(1)2. The structure is described by a herring-bone close-packing, along the a and b directions, of layers within which intermolecular N-H...pi and C-H...pi interactions can be found.
引用
收藏
页码:O910 / O912
页数:3
相关论文
共 13 条
[1]   SIR92 - a program for automatic solution of crystal structures by direct methods [J].
ALTOMARE, A ;
CASCARANO, G ;
GIACOVAZZO, G ;
GUAGLIARDI, A ;
BURLA, MC ;
POLIDORI, G ;
CAMALLI, M .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1994, 27 :435-435
[2]   AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY [J].
BLESSING, RH .
ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :33-38
[3]  
*BRUK AXS INC, 2001, SHELXTL VERS 6 12
[4]   ON ENANTIOMORPH-POLARITY ESTIMATION [J].
FLACK, HD .
ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881
[5]  
GRIDUNOVA GV, 1982, KRISTALLOGRAFIYA+, V27, P477
[6]   (η3-allyl)[(S)-(+)-(2-pyrrolidinylmethyl)pyrrolidine]palladium(II) trifluoromethanesulfonate [J].
Jones, MD ;
Paz, FAA ;
Davies, JE ;
Johnson, BFG .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 :M105-M107
[7]   [1,1′-bis(diphenylphosphino)ferrocene-κ2P,P′](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate dichloromethane disolvate [J].
Jones, MD ;
Paz, FAA ;
Davies, JE ;
Johnson, BFG .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :M111-M113
[8]   [(R)-(+)-1,1-Binaphthyl-2,2′-diamine](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate diethyl ether disolvate [J].
Jones, MD ;
Paz, FAA ;
Davies, JE ;
Johnson, BFG .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :M6-M7
[9]   Asymmetric activation of the Pd catalyst bearing the Tropos biphenylphosphine (BIPHEP) ligand with the chiral diaminobinaphthyl (DABN) activator [J].
Mikami, K ;
Aikawa, K ;
Yusa, Y .
ORGANIC LETTERS, 2002, 4 (01) :95-97
[10]   Dynamic asymmetric catalysis by diphenylphosphinoferrocene (DPPF)-nickel complexes through control of axial chirality by chiral diamines [J].
Mikami, K ;
Alkawa, K .
ORGANIC LETTERS, 2002, 4 (01) :99-101