Protection of a protecting Group: Preparation of stable N-silylated t-butyl carbamates

被引:18
作者
Roby, J [1 ]
Voyer, N [1 ]
机构
[1] UNIV SHERBROOKE,DEPT CHIM,SHERBROOKE,PQ J1K 2R1,CANADA
关键词
D O I
10.1016/S0040-4039(96)02271-X
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
The practical preparation of N-silylated carbamates (typified by 1) is reported. These compounds are synthesized in high yields by treating N-t-Boc-protected primary amines with silyl triflate reagents in dichloromethane in the presence of triethylamine. Copyright (C) 1996 Elsevier Science Ltd
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页码:191 / 194
页数:4
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