Quantitative RP-HPLC determination of some aldehydes and hydroxyaldehydes as their 2,4-dinitrophenylhydrazone derivatives

被引：43

作者：

Koivusalmi, E ^{[1
]}

Haatainen, E ^{[1
]}

Root, A ^{[1
]}

机构：

[1] NESTE OY, Corp Technol, Analyt Res, FIN-06101 Porvoo, Finland

来源：

ANALYTICAL CHEMISTRY | 1999年 / 71卷 / 01期

关键词：

D O I：

10.1021/ac980699f

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A high-performance liquid chromatographic (HPLC) method is described for the quantitative determination of some aliphatic aldehydes and beta-hydroxyaldehydes as their 2,4-dinitrophenylhydrazone derivatives. A method is described for the preparation of derivatives for those beta-hydroxyaldehydes where no reference compounds of known purity are available. The detection limit of the method was 4.3-21.0 mu g/L, depending on the aldehyde.

引用

页码：86 / 91

页数：6

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