Quantitative RP-HPLC determination of some aldehydes and hydroxyaldehydes as their 2,4-dinitrophenylhydrazone derivatives

被引：43

作者：

Koivusalmi, E ^{[1
]}

Haatainen, E ^{[1
]}

Root, A ^{[1
]}

机构：

[1] NESTE OY, Corp Technol, Analyt Res, FIN-06101 Porvoo, Finland

来源：

ANALYTICAL CHEMISTRY | 1999年 / 71卷 / 01期

关键词：

D O I：

10.1021/ac980699f

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A high-performance liquid chromatographic (HPLC) method is described for the quantitative determination of some aliphatic aldehydes and beta-hydroxyaldehydes as their 2,4-dinitrophenylhydrazone derivatives. A method is described for the preparation of derivatives for those beta-hydroxyaldehydes where no reference compounds of known purity are available. The detection limit of the method was 4.3-21.0 mu g/L, depending on the aldehyde.

引用

页码：86 / 91

页数：6

共 31 条

[11] PHOTOCHEMICAL FORMATION OF GLYOXYLIC AND PYRUVIC ACIDS IN SEAWATER [J].

KIEBER, DJ ;

MOPPER, K .

MARINE CHEMISTRY, 1987, 21 (02) :135-149

[12]

KING EP, 1958, J AM STAT ASSOC, V48, P531

[13] O-ALKYLOXIME DERIVATIVES FOR GAS-CHROMATOGRAPHIC AND GAS CHROMATOGRAPHIC-MASS SPECTROMETRIC DETERMINATION OF ALDEHYDES [J].

LEVINE, SP ;

HARVEY, TM ;

WAEGHE, TJ ;

SHAPIRO, RH .

ANALYTICAL CHEMISTRY, 1981, 53 (06) :805-809

[14] DETERMINATION OF FORMALDEHYDE IN CLEAN-AIR [J].

LOWE, DC ;

SCHMIDT, U ;

EHHALT, DH ;

FRISCHKORN, CGB ;

NURNBERG, HW .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1981, 15 (07) :819-823

[15] GAS-CHROMATOGRAPHY OF SIMPLE MONOCARBONYLS IN CIGARETTE WHOLE SMOKE AS THE BENZYLOXIME DERIVATIVES [J].

MAGIN, DF .

JOURNAL OF CHROMATOGRAPHY, 1980, 202 (02) :255-261

[16] PREPARATION AND GAS-CHROMATOGRAPHIC CHARACTERIZATION OF BENZYLOXIMES AND PARA-NITROBENZYLOXIMES OF SHORT-CHAIN (C1-C7) CARBONYLS [J].

MAGIN, DF .

JOURNAL OF CHROMATOGRAPHY, 1979, 178 (01) :219-227

[17] STUDIES ON STEROIDS .103. NEW TYPE OF DERIVATIVE FOR ELECTRON CAPTURE GAS CHROMATOGRAPHY OF KETOSTEROIDS [J].

NAMBARA, T ;

KIGASAWA, K ;

IWATA, T ;

IBUKI, M .

JOURNAL OF CHROMATOGRAPHY, 1975, 114 (01) :81-86

[18] GAS-CHROMATOGRAPHIC DETERMINATION OF HYDROXYPIVALALDEHYDE AS OXIME-TMS-DERIVATIVE [J].

OESTERHELT, G ;

POZEG, M ;

BUBENDORF, A ;

BARTOLDUS, D .

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1985, 321 (06) :553-555

[19] DETECTION OF INDIVIDUAL CARBON RESONANCES IN SOLID PROTEINS [J].

OPELLA, SJ ;

FREY, MH ;

CROSS, TA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1979, 101 (19) :5856-5857

[20] CHROMATOGRAPHIC DETERMINATION OF CARBONYL-COMPOUNDS AS THEIR 2,4-DINITROPHENYLHYDRAZONES .2. HIGH-PRESSURE LIQUID CHROMATOGRAPHY [J].

PAPA, LJ ;

TURNER, LP .

JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1972, 10 (12) :747-750

← 1 2 3 4 →