Study of heterogeneous properties of solids by means of a special thermal analysis technique

被引：8

作者：

Staszczuk, P ^{[1
]}

Glazewski, D ^{[1
]}

机构：

[1] Marie Curie Sklodowska Univ, Fac Chem, Inst Phys Chem, Dept Physicochem Solid Surfaces, PL-20031 Lublin, Poland

来源：

JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 1999年 / 55卷 / 02期

关键词：

heterogeneity of solids; quasi-isothermal technique; thermodesorption of liquids;

D O I：

10.1023/A:1010119719085

中图分类号：

O414.1 [热力学];

学科分类号：

摘要：

Thermogravimetry (TG) was successfully applied in order to study the heterogeneous properties of solid surfaces and adsorbed liquid films. The method utilized the thermogravimetric mass-loss Q-TG and differential Q-DTG curves with respect to temperature and pra time for the desorption of liquidus from solid surfaces under quasi-isothermal conditions. Evaluation of the experimental data revealed the heterogeneous properties of the tested samples. It appears that this modern special TG technique is very useful for the study of liquid/solid systems and can be competitive with traditional techniques because of the speed and accuracy with which the data are obtained and the simplicity of the experimental operations.

引用

页码：467 / 481

页数：15

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