Diffraction effects in inner-shell ionization edges

被引:19
作者
Schattschneider, P [1 ]
Nelhiebel, M [1 ]
Schenner, M [1 ]
Grogger, W [1 ]
Hofer, F [1 ]
机构
[1] GRAZ TECH UNIV, FORSCHUNGSINST ELEKTRONENMIKROSKOPIE & FEINSTRUKT, A-8010 GRAZ, AUSTRIA
关键词
electron energy-loss spectrometry; EELS; crystal; Bragg scattering; inelastic electron scattering; core loss;
D O I
10.1046/j.1365-2818.1996.73076.x
中图分类号
TH742 [显微镜];
学科分类号
摘要
The influences of elastic on inelastic scattering under systematic-row conditions are described in a simple way. A kinematic approach, superposing inelastic intensity-distribution profiles centered at different Bragg spots is shown to be qualitatively correct but quantitatively unsatisfying. A model considering Bragg reflection of the fast electron before and after the inelastic scattering process and thus introducing interference effects is in good agreement with experimental results. Experimentally, we recorded inelastic intensities in the diffraction pattern of an epitaxial copper foil using a PEELS spectrometer and observed energy filtered extinction contours of a copper crystal.
引用
收藏
页码:18 / 26
页数:9
相关论文
共 24 条
[1]   ELECTRON-ENERGY LOSS SPECTROSCOPY IN A CRYSTALLINE ENVIRONMENT USING INNER-SHELL IONIZATION [J].
ALLEN, LJ .
ULTRAMICROSCOPY, 1993, 48 (1-2) :97-106
[2]   SYMMETRY-SELECTED ELECTRON-ENERGY-LOSS SCATTERING IN DIAMOND [J].
BATSON, PE .
PHYSICAL REVIEW LETTERS, 1993, 70 (12) :1822-1825
[3]   EXPERIMENTAL ENERGY-LOSS FUNCTION, IM[-1/EPSILON(Q,OMEGA)], FOR ALUMINUM [J].
BATSON, PE ;
SILCOX, J .
PHYSICAL REVIEW B, 1983, 27 (09) :5224-5239
[4]   PHASE DEPENDENCE OF KIKUCHI PATTERNS .1. THEORY [J].
BIRD, DM ;
WRIGHT, AG .
ACTA CRYSTALLOGRAPHICA SECTION A, 1989, 45 :104-109
[5]   DYNAMICAL TREATMENT OF KIKUCHI PATTERNS [J].
CHUKHOVSKII, FN ;
ALEXANJA.LA ;
PINSKER, ZG .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 1973, 29 (JAN1) :38-45
[6]   MEASUREMENT OF INELASTIC ELECTRON-SCATTERING CROSS-SECTIONS BY ELECTRON ENERGY-LOSS SPECTROSCOPY [J].
CROZIER, PA .
PHILOSOPHICAL MAGAZINE B-PHYSICS OF CONDENSED MATTER STATISTICAL MECHANICS ELECTRONIC OPTICAL AND MAGNETIC PROPERTIES, 1990, 61 (03) :311-336
[7]   MULTIPLE LEAST-SQUARES FITTING FOR QUANTITATIVE ELECTRON-ENERGY-LOSS SPECTROSCOPY - AN EXPERIMENTAL INVESTIGATION USING STANDARD SPECIMENS [J].
DOOR, R ;
GANGLER, D .
ULTRAMICROSCOPY, 1995, 58 (02) :197-210
[8]  
Egerton R.F., 2011, Electron Energy-loss Spectroscopy in the Electron Microscope, Vthird, DOI DOI 10.1007/978-1-4419-9583-4
[9]  
Hirsch, 1965, ELECT MICROSCOPY THI
[10]  
HOFER F, 1994, ENERGY FILTERING TRA, P225