Characterization of chitin from Illex argentinus squid pen

被引:78
作者
Cortizo, M. Susana [3 ]
Berghoff, Carla F. [3 ,4 ]
Alessandrini, Jose Luis [1 ,2 ,4 ]
机构
[1] UNLP, Dept Fis, Fac Ciencias Exactas, RA-1900 La Plata, Buenos Aires, Argentina
[2] IFLP, RA-1900 La Plata, Buenos Aires, Argentina
[3] UNLP, INIFTA, Fac Ciencias Exactas, RA-1900 La Plata, Argentina
[4] Comis Invest Cient Prov Buenes Aires, RA-1900 La Plata, Buenos Aires, Argentina
关键词
chitin; Illex argentinus; NMR; molecular weight; viscosity; persistence length;
D O I
10.1016/j.carbpol.2008.01.004
中图分类号
O69 [应用化学];
学科分类号
081704 [应用化学];
摘要
beta-Chitin from Illex argentinus squid pens was isolated by using chemical methods and the pens composition determined. The structural characteristics of beta-chitin were identified with infrared (IR), solid-state cross-polarization/magic-angle-spinning (CP-MAS) C-13 NMR spectroscopy and X-ray analysis. The viscosity average molecular weight M-v, calculated from the intrinsic viscosity was above 2 x 10(6) g mol(-1). The stiffness of the macromolecule was analyzed using the Yamakawa and Fujii theory for wormlike cylinders. (c) 2008 Elsevier Ltd. All rights reserved.
引用
收藏
页码:10 / 15
页数:6
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