Phenol solvothermal synthesis of JBW-type zeolites

被引:7
作者
Bo, Wei [1 ]
Ye, Wang
Ming-hong, Xin
Shi-lun, Qiu
机构
[1] Shenzhen Univ, Chem & Chem Engn Coll, Shenzhen 518060, Peoples R China
[2] Xiamen Univ, State Key Lab Phys Chem Solid Surfaces, Xiamen 361005, Peoples R China
[3] Jilin Univ, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130021, Peoples R China
关键词
JBW; phenol; solvothermal synthesis; aluminosilicate;
D O I
10.1016/S1005-9040(07)60111-1
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Phenol was used as an aromatic and acidic solvent in solvothermal synthesis. JRW- type zeolites were successfully synthesized in a phenolic system. The as-synthesized microporous crystals were characterized by powder X-ray diffraction analysis and scanning electron microscopy techniques. The results indicate that phenol is a good organic solvent and has a huge potential of application in studying crystallization mechanism and synthesizing novel microporous materials.
引用
收藏
页码:511 / 513
页数:3
相关论文
共 19 条
[11]  
RHEINHARDT A, 1982, FORTSCH MINERALOGIE, V60, P175
[12]  
Sheldrick W. S., 1997, ANGEW CHEM INT EDIT, V36, P206
[13]   Solvothermal syntheses, crystal structures, and thermal stability of two new thioantimonates(III) using complex transition metal cations as structure directing agents:: the layered compound [Ni(dien)2]Sb4S7•H2O and the three-dimensional compound [Ni(dien)2]3Sb12S21•H2O [J].
Stähler, R ;
Näther, C ;
Bensch, W .
JOURNAL OF SOLID STATE CHEMISTRY, 2003, 174 (02) :264-275
[14]  
SUGIMOTO M, 1986, P 7 INT ZEOL C TOK, P193
[15]   Hydrothermal synthesis and structural characterization of the aluminogermanate analogues of JBW, montesommaite, analcime and paracelsian [J].
Tripathi, A ;
Parise, JB .
MICROPOROUS AND MESOPOROUS MATERIALS, 2002, 52 (02) :65-78
[16]   Solvothermal synthesis and structural characterization of a three-dimensional metal-organic polymer [NaZn(1,2,4-BTC)](1,2,4-BTC=1,2,4-benzenetricarboxylate) [J].
Wang, L ;
Shi, Z ;
Li, GH ;
Fan, Y ;
Fu, WS ;
Feng, SH .
SOLID STATE SCIENCES, 2004, 6 (01) :85-90
[17]   Three-dimensional open-framework nickel aluminophosphate [NiAlP2O8][C2N2H9]:: Assembly of one-dimensional AlP2O83- chains through [NiO5N] octahedra [J].
Wei, B ;
Yu, JH ;
Shi, Z ;
Qiu, SL ;
Yan, WF ;
Terasaki, O .
CHEMISTRY OF MATERIALS, 2000, 12 (08) :2065-2067
[18]   Solvothermal synthesis and characterization of a new 3-D open framework aluminophosphate [Al2P3O12][C4N3H16] [J].
Wei, B ;
Zhu, GS ;
Yu, JH ;
Qiu, SL ;
Xiao, FS ;
Terasaki, O .
CHEMISTRY OF MATERIALS, 1999, 11 (12) :3417-+
[19]   A benzene-thermal synthetic route to nanocrystalline GaN [J].
Xie, Y ;
Qian, YT ;
Wang, WZ ;
Zhang, SY ;
Zhang, YH .
SCIENCE, 1996, 272 (5270) :1926-1927