Porous silica of self-similar morphology

被引:8
作者
Aikawa, K
Kaneko, K
Fujitsu, M
Tamura, T
Ohbu, K
机构
[1] Chiba Univ, Fac Sci, Dept Chem, Inage Ku, Chiba 263, Japan
[2] Lion Corp, Mat Sci Res Ctr, Edogawa Ku, Tokyo 132, Japan
关键词
D O I
10.1021/la9710031
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
New mesoporous silica was prepared using the template of the bicontinuous layered structure from the bicontinuous phase of poly(oxyethylene) dodecyl ether, H2O, and isooctane and the aqueous phase of 6 N HCl and teraethoxysilane. The synthesized silica was characterized by scanning electron microscopy (SEM) observation, X-ray diffraction, small angle X-ray scattering (SAXS), mercury porosimetry, and N-2 adsorption at 77 K. The structure had a fractal nature of which cluster fractal dimensions are 1.7 and 1.83 from SEM observation and SAXS, respectively. The silica structure was noncrystalline like MCM-41. The prepared silica was highly porous and had a wide range pores from ultramicropores to macropores.
引用
收藏
页码:3041 / 3044
页数:4
相关论文
共 24 条
[1]   CHEMISTRY IN NONINTEGER DIMENSIONS BETWEEN 2 AND 3 .2. FRACTAL SURFACES OF ADSORBENTS [J].
AVNIR, D ;
FARIN, D ;
PFEIFER, P .
JOURNAL OF CHEMICAL PHYSICS, 1983, 79 (07) :3566-3571
[2]  
Avnir D., 1989, The Fractal Approach to Heterogeneous Chemistry: Surfaces, Colloids, Polymers
[3]   A NEW FAMILY OF MESOPOROUS MOLECULAR-SIEVES PREPARED WITH LIQUID-CRYSTAL TEMPLATES [J].
BECK, JS ;
VARTULI, JC ;
ROTH, WJ ;
LEONOWICZ, ME ;
KRESGE, CT ;
SCHMITT, KD ;
CHU, CTW ;
OLSON, DH ;
SHEPPARD, EW ;
MCCULLEN, SB ;
HIGGINS, JB ;
SCHLENKER, JL .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (27) :10834-10843
[4]   ANALYSIS OF NITROGEN ADSORPTION ISOTHERMS ON POROUS AND NONPOROUS SILICAS BY BET AND ALPHAS METHODS [J].
BHAMBHANI, MR ;
TURK, DH ;
SING, KSW ;
CUTTING, PA .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1972, 38 (01) :109-+
[5]  
DOLLIMORE D, 1964, J APPL CHEM, V14, P109
[6]  
Gregg S. J., 1982, ADSORPTION SURFACE A, P287
[7]   Mechanical stability of pure silica mesoporous MCM-41 by nitrogen adsorption and small-angle X-ray diffraction measurements [J].
Gusev, VY ;
Feng, XB ;
Bu, Z ;
Haller, GL ;
OBrien, JA .
JOURNAL OF PHYSICAL CHEMISTRY, 1996, 100 (06) :1985-1988
[8]   GENERALIZED SYNTHESIS OF PERIODIC SURFACTANT INORGANIC COMPOSITE-MATERIALS [J].
HUO, QS ;
MARGOLESE, DI ;
CIESLA, U ;
FENG, PY ;
GIER, TE ;
SIEGER, P ;
LEON, R ;
PETROFF, PM ;
SCHUTH, F ;
STUCKY, GD .
NATURE, 1994, 368 (6469) :317-321
[9]   HELICAL MICROTUBULES OF GRAPHITIC CARBON [J].
IIJIMA, S .
NATURE, 1991, 354 (6348) :56-58
[10]   AN ORDERED WATER MOLECULAR ASSEMBLY STRUCTURE IN A SLIT-SHAPED CARBON NANOSPACE [J].
IIYAMA, T ;
NISHIKAWA, K ;
OTOWA, T ;
KANEKO, K .
JOURNAL OF PHYSICAL CHEMISTRY, 1995, 99 (25) :10075-10076