Eco-friendly and efficient one-pot synthesis of alkyl- or aryl-14H-dibenzo[a,j]xanthenes in water

被引:113
作者
Dabiri, Minoo [1 ]
Baghbanzadeh, Mostafa [1 ]
Nikcheh, Maryam Shakouri [1 ]
Arzroomchilar, Elham [1 ]
机构
[1] Shahid Beheshti Univ, Fac Sci, Dept Chem, Tehran, Iran
关键词
D O I
10.1016/j.bmcl.2007.07.008
中图分类号
R914 [药物化学];
学科分类号
100701 ;
摘要
Alkyl- or aryl-14H-dibenzo[a,j]xanthene derivatives are synthesized efficiently by the reaction of P-naphthol and aliphatic and aromatic aldehydes in the presence of KA1(SO4)(2).12H(2)O (alum) under aqueous condition at 100 degrees C. Different types of aromatic and aliphatic aldehydes are used in the reaction and in all cases the products synthesized successfully. Several solvents were examined for this reaction; however, in terms of reaction yield and time, water was found to be the optimum solvent. (c) 2007 Elsevier Ltd. All rights reserved.
引用
收藏
页码:436 / 438
页数:3
相关论文
共 33 条
[1]   Method for the analysis of phloxine B, uranine, and related xanthene dyes in soil using supercritical fluid extraction and high performance liquid chromatography [J].
AlcantaraLicudine, JP ;
Kawate, MK ;
Li, QX .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (03) :766-773
[2]   Water-accelerated synthesis of novel bis-2,3-dihydroquinazolin-4(1H)-one derivatives [J].
Baghbanzadeh, M ;
Salehi, P ;
Dabiri, M ;
Kozeligarya, G .
SYNTHESIS-STUTTGART, 2006, (02) :344-348
[3]   CHEMICAL ASPECTS OF SANTALIN AS A HISTOLOGICAL STAIN [J].
BANERJEE, A ;
MUKHERJEE, AK .
STAIN TECHNOLOGY, 1981, 56 (02) :83-85
[4]   NEW TOTAL SYNTHESIS OF BIKAVERIN [J].
BEKAERT, A ;
ANDRIEUX, J ;
PLAT, M .
TETRAHEDRON LETTERS, 1992, 33 (20) :2805-2806
[5]   One-pot synthesis of mono- and disubstituted (3H)-quinazolin-4-ones in dry media under microwave irradiation [J].
Dabiri, M ;
Salehi, P ;
Mohammadi, AA ;
Baghbanzadeh, M .
SYNTHETIC COMMUNICATIONS, 2005, 35 (02) :279-287
[6]   Efficient synthesis of mono- and disubstituted 2,3-dihydroquinazolin-4(1H)-ones using KAl(SO4)2•12H2O as a reusable catalyst in water and ethanol [J].
Dabiri, M ;
Salehi, P ;
Otokesh, S ;
Baghbanzadeh, M ;
Kozehgary, G ;
Mohammadi, AA .
TETRAHEDRON LETTERS, 2005, 46 (36) :6123-6126
[7]  
Dabiri M, 2004, J CHEM RES-S, P570
[8]   Silica sulfuric acid: An efficient and versatile acidic catalyst for the rapid and ecofriendly synthesis of 1,3,4-oxadiazoles at ambient temperature [J].
Dabiri, Minoo ;
Salehi, Peyman ;
Baghbanzadeh, Mostafa ;
Zolfigol, Mohammad Ali ;
Bahramnejad, Mahboobeh .
SYNTHETIC COMMUNICATIONS, 2007, 37 (7-9) :1201-1209
[9]   Diammonium hydrogen phosphate as an efficient and inexpensive catalyst for the synthesis of bis(indolyl)methanes under solvent-free conditions [J].
Dabiri, Minoo ;
Salehi, Peyman ;
Baghbanzadeh, Mostafa ;
Vakilzadeh, Yasamin ;
Kiani, Shadi .
MONATSHEFTE FUR CHEMIE, 2007, 138 (06) :595-597
[10]   Silica sulfuric acid as an efficient and reusable catalyst for the pechmann synthesis of coumarins under solvent-free conditions [J].
Dabiri, Minoo ;
Salehi, Peyman ;
Zolfigol, Mohammad Ali ;
Baghbanzadeh, Mostafa .
HETEROCYCLES, 2007, 71 (03) :677-682