Synthesis of Silver Nanoparticles in Chitosan, Gelatin and Chitosan/Gelatin Bionanocomposites by a Chemical Reducing Agent and Their Characterization

被引:184
作者
Bin Ahmad, Mansor [1 ]
Lim, Jenn Jye [1 ]
Shameli, Kamyar [1 ]
Ibrahim, Nor Azowa [1 ]
Tay, Mei Yen [1 ]
机构
[1] Univ Putra Malaysia, Fac Sci, Dept Chem, Upm Serdang 43400, Selangor, Malaysia
关键词
chitosan; gelatin; silver; bionanocomposite; chemical reduction method; SIZE-CONTROLLED SYNTHESIS; GOLD; NANOCOMPOSITES; FTIR;
D O I
10.3390/molecules16097237
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
070307 [化学生物学]; 071010 [生物化学与分子生物学];
摘要
In this research, silver nanoparticles (AgNPs) were synthesized in chitosan (Cts), Cts/gelatin and gelatin suspensions using a chemical reducing agent. Cts and gelatin were used as natural stabilizers and solid support, whereas AgNO3 was used as the silver precursor. Sodium borohydride (NaBH4) was used as the reducing agent. The properties of AgNPs in Cts, Cts/gelatin and gelatin bionanocomposites (BNCs) were studied in terms of their surface plasmon resonance, crystalline structure, average diameter size, particle distributions, surface topography and functional groups. All the samples were characterized by UV-visible spectroscopy, powder X-ray diffraction, transmission electron microscopy, atomic force microscopy and Fourier transform infrared spectroscopy.
引用
收藏
页码:7237 / 7248
页数:12
相关论文
共 31 条
[1]
Ahmad M.B., 2009, Am. J. Appl. Sci, V6, P2030, DOI DOI 10.3844/AJASSP.2009.2030.2035
[2]
Preparation and characterization of gold and silver nanoparticles in layered Laponite suspensions [J].
Aihara, N ;
Torigoe, K ;
Esumi, K .
LANGMUIR, 1998, 14 (17) :4945-4949
[3]
Bin Ahmad Mansor, 2009, American Journal of Applied Sciences, V6, P1909, DOI 10.3844/ajassp.2009.1909.1914
[4]
Preparation of silver nanoparticles with antimicrobial activities and the researches of their biocompatibilities [J].
Cao, X. L. ;
Cheng, C. ;
Ma, Y. L. ;
Zhao, C. S. .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN MEDICINE, 2010, 21 (10) :2861-2868
[5]
Key factors in chemical reduction by hydrazine for recovery of precious metals [J].
Chen, JP ;
Lim, LL .
CHEMOSPHERE, 2002, 49 (04) :363-370
[6]
Cheng J., 2006, FRONT CHEM CHINA, V1, P418, DOI 10.1007/s11458-006-0067-0
[7]
Chitosan-clay nanocomposites: application as electrochemical sensors [J].
Darder, M ;
Colilla, M ;
Ruiz-Hitzky, E .
APPLIED CLAY SCIENCE, 2005, 28 (1-4) :199-208
[8]
Synthesis and characterization of UV-irradiated silver/montmorillonite nanocomposites [J].
Darroudi, Majid ;
Bin Ahmad, Mansor ;
Shameli, Kamyar ;
Abdullah, Abdul Halim ;
Ibrahim, Nor Azowa .
SOLID STATE SCIENCES, 2009, 11 (09) :1621-1624
[9]
Photochemical Strategies for the Facile Synthesis of Gold-Silver Alloy and Core-Shell Bimetallic Nanoparticles [J].
Gonzalez, Carlos Miguel ;
Liu, Yun ;
Scaiano, J. C. .
JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 113 (27) :11861-11867
[10]
Preparation and characterization of stable monodisperse silver nanoparticles via photoreduction [J].
Guang-nian, Xu ;
Xue-liang, Qiao ;
Xiao-lin, Qiu ;
Jian-guo, Chen .
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2008, 320 (1-3) :222-226