Analysis of polycyclic aromatic hydrocarbons in airborne particles using open-vessel focused microwave-assisted extraction

被引：27

作者：

Shu, YY ^{[1
]}

Tey, SY ^{[1
]}

Wu, DKS ^{[1
]}

机构：

[1] Natl Kaohsiung Normal Univ, Dept Chem, Kaohsiung, Taiwan

来源：

ANALYTICA CHIMICA ACTA | 2003年 / 495卷 / 1-2期

关键词：

focused microwave-assisted extraction; open-vessel; polycyclic aromatic hydrocarbon; urban dust reference material; airborne particle;

D O I：

10.1016/j.aca.2003.08.040

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A procedure to extract polycyclic aromatic hydrocarbons (PAHs) from airborne particles using open-vessel focused microwave-assisted extraction (FMAE) is proposed. Parameters which might affect extraction efficiency such as solvent composition, extraction time, microwave power, and sample water addition were investigated. Recoveries for PAHs from urban dust standard reference material (SRM) 1649a were between 77 and 116% with relative standard deviations between 2 and 18% on the basis of certified values by using an optimized condition: in a 20ml 5% acetone in toluene at 150W of microwave power for 20 min extraction. The optimized FMAE condition was compared to Soxhlet method on the extraction of standard reference material and real particulate air samples collected from urban area. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：99 / 108

页数：10

共 52 条

[1]

[Anonymous], SPECTROSC INT J

[2]

BACK SO, 1991, WATER AIR SOIL POLL, V60, P273

[3] Optimisation of the microwave-assisted extraction in open cell of polycyclic aromatic hydrocarbons from soils and sediments - Study of moisture effect [J].

Budzinski, H ;

Letellier, M ;

Garrigues, P ;

Le Menach, K .

JOURNAL OF CHROMATOGRAPHY A, 1999, 837 (1-2) :187-200

[4] Microwave-assisted solvent extraction of environmental samples [J].

Camel, V .

TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2000, 19 (04) :229-248

[5] Focused microwave assistance for extracting some pesticide residues from strawberries into water before their determination by SPME/HPLC/DAD [J].

Cao, CF ;

Wang, Z ;

Urruty, L ;

Pommier, JJ ;

Montury, M .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2001, 49 (11) :5092-5097

[6] Determination of organotin compounds by liquid chromatography-inductively coupled plasma mass spectrometry with a direct injection nebulizer [J].

Chao, WS ;

Jiang, SJ .

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1998, 13 (12) :1337-1341

[7] Seasonal variation of fractures of the hip in elderly persons [J].

Chiu, KY ;

Ng, TP ;

Chow, SP .

INJURY-INTERNATIONAL JOURNAL OF THE CARE OF THE INJURED, 1996, 27 (05) :333-336

[8] ANALYSIS OF POLYCYCLIC AROMATIC-HYDROCARBONS IN AIR PARTICULATE MATTER FROM A LIGHTLY INDUSTRIALIZED URBAN AREA [J].

CRETNEY, JR ;

LEE, HK ;

WRIGHT, GJ ;

SWALLOW, WH ;

TAYLOR, MC .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1985, 19 (05) :397-404

[9] Optimisation of the extraction of arsenic species from mussels with low power focused microwaves by applying a Doehlert design [J].

Dagnac, T ;

Padró, A ;

Rubio, R ;

Rauret, G .

ANALYTICA CHIMICA ACTA, 1998, 364 (1-3) :19-30

[10] DETERMINATION OF TRIALKYL AND TRIARYL PHOSPHATES IN SEDIMENT USING MICROWAVE EXTRACTION AND PACKED-CAPILLARY SUPERCRITICAL-FLUID CHROMATOGRAPHY [J].

DEGEUS, H ;

ZEGERS, BN ;

LINGEMAN, H ;

BRINKMAN, UAT .

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1994, 56 (02) :119-132

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