Solid state NMR, X-ray diffraction, and infrared characterization of local structure in heat-treated oxyhydroxyapatite microcrystals:: An analog of the thermal decomposition of hydroxyapatite during plasma-spray procedure

被引:47
作者
Hartmann, P
Jäger, C
Barth, S
Vogel, J
Meyer, K
机构
[1] Univ Jena, Inst Opt & Quantenelekt, D-07743 Jena, Germany
[2] Hermsdorfer Inst Techn Keram, D-07629 Hermsdorf, Germany
[3] Univ Jena, Otto Schott Inst, D-07743 Jena, Germany
[4] Univ Jena, Inst Phys Chem, D-07743 Jena, Germany
关键词
hydroxyapatite; solid state nuclear magnetic resonance; IR spectroscopy;
D O I
10.1006/jssc.2001.9274
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The structure of plasma-sprayed hydroxyapatites possesses a variety of partially dehydrated hydroxyapatite structures. Nuclear magnetic resonance, IR spectroscopy, and X-ray diffraction have been used to analyze the structure of partially dehydrated hydroxyapatites. The oxyhydroxyapatites are prepared from crystalline hydroxyapatite by thermal treatment in air. The obtained results enable an advanced phase analysis of plasma-sprayed hydroxyapatite layers. (C) Academic Press.
引用
收藏
页码:460 / 468
页数:9
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