In situ templated synthesis of anatase single-crystal nanotube arrays

被引：105

作者：

Zhao, JL ^{[1
]}

Wang, XH ^{[1
]}

Sun, TY ^{[1
]}

Li, LT ^{[1
]}

机构：

[1] Tsing Hua Univ, Dept Mat Sci & Engn, State Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China

来源：

NANOTECHNOLOGY | 2005年 / 16卷 / 10期

关键词：

D O I：

10.1088/0957-4484/16/10/077

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Anatase single-crystal nanotubes were obtained using an in situ templated method. First, highly ordered titania arrays were formed through an anodization process in H3PO4 electrolytes containing 0.5 wt% HE Under optimized conditions titania nanotubes with a diameter of up to 100 nm and a length of up to 1.1 mu m were prepared. Second, the crystallization and stability of the titania nanotubes were studied in air at elevated temperatures. Anatase single-crystal nanotubes were fabricated after annealing the sample in air at 450 degrees C. The anatase single-crystal structure was verified by selected area diffraction pattern and HRTEM images.

引用

页码：2450 / 2454

页数：5

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