Field-portable, high-speed GC/TOFMS

被引:45
作者
Syage, JA [1 ]
Nies, BJ [1 ]
Evans, MD [1 ]
Hanold, KA [1 ]
机构
[1] Syagen Technol Inc, Tustin, CA 92780 USA
关键词
D O I
10.1016/S1044-0305(01)80210-5
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
This work is focused on developing a fast gas chromatograph, time-of-flight mass spectrometer (GC/TOFMS) for man-portable field use. The goal is to achieve a total system solution for meeting performance, size, weight, power, cost, and ruggedness requirements for a laboratory in the field. The core technology will also be adaptable to specific applications including real-time point detection for hazardous chemical releases (e.g., chemical weapons), for biological agent signature identification, and for mobile monitoring platforms (e.g., air, ship, truck). Previously we presented results of a feasibility demonstration for a 30-lb field-portable TOFMS system. In this work we present recent progress in integrating a low-power, high-speed GC and show the capability for accurately recording fast GC transients for targeted compound detection using a quadrupole ion trap, time-of-flight instrument (QitTof). (C) 2001 American Society for Mass Spectrometry.
引用
收藏
页码:648 / 655
页数:8
相关论文
共 15 条
[1]  
BAYKUT G, 1994, TRAC-TREND ANAL CHEM, V13, P267, DOI 10.1016/0165-9936(94)87063-2
[2]   High-order kinetic energy focusing in an end cap reflectron time-of-flight mass spectrometer [J].
Cornish, TJ ;
Cotter, RJ .
ANALYTICAL CHEMISTRY, 1997, 69 (22) :4615-4618
[3]  
Eckenrode BA, 1998, FIELD ANAL CHEM TECH, V2, P3, DOI 10.1002/(SICI)1520-6521(1998)2:1<3::AID-FACT2>3.0.CO
[4]  
2-Z
[5]   High-pressure effects in miniature arrays of quadrupole analyzers for residual gas analysis from 10(-9) to 10(-2) Torr [J].
Ferran, RJ ;
Boumsellek, S .
JOURNAL OF VACUUM SCIENCE & TECHNOLOGY A, 1996, 14 (03) :1258-1265
[6]  
Grob R.L., 1995, MODERN PRACTICE GAS
[7]  
Hart KJ, 2000, FIELD ANAL CHEM TECH, V4, P93, DOI 10.1002/1520-6521(2000)4:2/3<93::AID-FACT4>3.0.CO
[8]  
2-W
[9]  
MCDONALD WC, 1994, ENVIRON SCI TECHNOL, V28, pA336, DOI 10.1021/es00056a719
[10]   Miniature, high-resolution, quadrupole mass-spectrometer array [J].
Orient, OJ ;
Chutjian, A ;
Garkanian, V .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (03) :1393-1397