Combinatorial approach to characterizing epoxy curing

被引:32
作者
Eidelman, N
Raghavan, D
Forster, AM
Amis, EJ
Karim, A
机构
[1] Natl Inst Stand & Technol, Amer Dent Assoc Fdn, Paffenbarger Res Ctr, Gaithersburg, MD 20899 USA
[2] Howard Univ, Dept Chem, Washington, DC 20059 USA
[3] Natl Inst Stand & Technol, Div Polymers, Gaithersburg, MD 20899 USA
关键词
adhesion; confocal microscopy; curing; epoxy; FTIR microspectroscopy;
D O I
10.1002/marc.200300190
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
Three complementary techniques that probe different characteristics of curing: FTIR microspectroscopy, confocal microscopy and axisymmetric adhesion testing were used to study discrete epoxy samples cured at different temperatures and to follow curing across a continuous gradient combinatorial library. Together, these techniques provide a comprehensive picture of chemical and physical changes.
引用
收藏
页码:259 / 263
页数:5
相关论文
共 37 条
[1]   Effects of substrate modification on the interfacial adhesion of acrylic elastomers [J].
Ahn, D ;
Shull, KR .
LANGMUIR, 1998, 14 (13) :3646-3654
[2]   Study of a curing reaction of an epoxy resin [J].
Barbadillo, F ;
Losada, R ;
Suárez, M ;
Mier, JL ;
García, L ;
Naya, S .
THERMEC'2003, PTS 1-5, 2003, 426-4 :2163-2168
[3]   White matter changes and cognitive performance in aging [J].
Bartrés-Faz, B ;
Clemente, IC ;
Junqué, C .
REVISTA DE NEUROLOGIA, 2001, 33 (04) :347-353
[4]   Combinatorial measurements of crystallization growth rate and morphology in thin films of isotactic polystyrene [J].
Beers, KL ;
Douglas, JF ;
Amis, EJ ;
Karim, A .
LANGMUIR, 2003, 19 (09) :3935-3940
[5]   Specular reflectance: A convenient tool for polymer characterisation by FTIR-microscopy? [J].
Chalmers, JM ;
Everall, NJ ;
Ellison, S .
MICRON, 1996, 27 (05) :315-328
[6]   CORRELATION BETWEEN ADHESION HYSTERESIS AND PHASE STATE OF MONOLAYER FILMS [J].
CHAUDHURY, MK ;
OWEN, MJ .
JOURNAL OF PHYSICAL CHEMISTRY, 1993, 97 (21) :5722-5726
[7]  
CHU FDJ, 1995, J ADHESION, V53, P149
[8]  
Crosby AJ, 1999, J POLYM SCI POL PHYS, V37, P3455, DOI 10.1002/(SICI)1099-0488(19991215)37:24<3455::AID-POLB7>3.0.CO
[9]  
2-3
[10]   Combinatorial investigations of interfacial failure [J].
Crosby, AJ ;
Karim, A ;
Amis, EJ .
JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 2003, 41 (09) :883-891