Syntheses of TiO2(B) nanowires and TiO2 anatase nanowires by hydrothermal and post-heat treatments

被引：267

作者：

Yoshida, R ^{[1
]}

Suzuki, Y ^{[1
]}

Yoshikawa, S ^{[1
]}

机构：

[1] Kyoto Univ, Inst Adv Energy, Uji, Kyoto 6110011, Japan

来源：

JOURNAL OF SOLID STATE CHEMISTRY | 2005年 / 178卷 / 07期

关键词：

hydrothermal process; TiO2(B) nanowim anatase nanowire; microstructure;

D O I：

10.1016/j.jssc.2005.04.025

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

TiO2(B) nanowires and TiO2 anatase nanowires were synthesized by the hydrothermal processing in 10 M NaOH aq. at 150 degrees C followed by the post-heat treatment at 300-800 degrees C. As-synthesized Na-free titanate nanowires (prepared by the hydrothermal treatment and repeated ion exchanging by HCl (aq.) were transformed into TiO2(B) structure with maintaining 1-D morphology at 300-500 degrees C, and further transformed into anatase structure at 600-800 degrees C with keeping 1-D shape. At 900 degrees C, they transformed into rod-shaped rutile grains. Microstructure of these 1-D TiO2 nanomaterials is reported. (c) 2005 Elsevier Inc. All rights reserved.

引用

页码：2179 / 2185

页数：7

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