Influence of ethanol content in the precipitation medium on the composition, structure and reactivity of magnesium-calcium phosphate

被引:18
作者
Babaie, Elham [1 ]
Zhou, Huan [2 ]
Lin, Boren [1 ]
Bhaduri, Sarit B. [3 ,4 ]
机构
[1] Univ Toledo, Dept Bioengn, Toledo, OH 43606 USA
[2] Changzhou Univ, Inst Biomed Engn & Hlth Sci, Changzhou, Jiangsu, Peoples R China
[3] Univ Toledo, Dept Mech Ind & Mfg Engn, Toledo, OH 43606 USA
[4] Univ Toledo, Dept Surg Dent, Toledo, OH 43606 USA
来源
MATERIALS SCIENCE AND ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS | 2015年 / 53卷
关键词
Amorphous phase; Magnesium phosphate; Calcium phosphate; Ethanol; STRUVITE; PH;
D O I
10.1016/j.msec.2015.04.011
中图分类号
TB3 [工程材料学]; R318.08 [生物材料学];
学科分类号
082905 [生物质能源与材料]; 100103 [病原生物学];
摘要
Biocompatible amorphous magnesium calcium phosphate (AMCP) particles were synthesized using ethanol in precipitation medium from moderately supersaturated solution at pH 10. Some synthesis parameters such as, (Mg + Ca):P, Mg:Ca ratio and different drying methods on the structure and stability of as-produced powder was studied and characterized using SEM, XRD and cell cytocompatibility. The results showed that depending on the Mg2+ concentration, nano crystalline Struvite (MgNH4PO4 center dot 6H(2)O) can also be alternatively formed. However, the as-formed AMCP preserved its amorphous structure after 7 days of incubation in SBF for tested phosphate concentration, and equally ionic concentration of magnesium and calcium. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:204 / 211
页数:8
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