Design and performance of a microcantilever-based hydrogen sensor

被引:177
作者
Baselt, DR
Fruhberger, B
Klaassen, E
Cemalovic, S
Britton, CL
Patel, SV
Mlsna, TE
McCorkle, D
Warmack, B
机构
[1] Graviton Inc, Chem Sensors Div, La Jolla, CA 92037 USA
[2] Oak Ridge Natl Lab, Oak Ridge, TN 37831 USA
[3] Intel Corp, Santa Clara, CA 95052 USA
关键词
hydrogen; cantilever; palladium; MEMS; gas sensor;
D O I
10.1016/S0925-4005(02)00315-5
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This paper describes the design of, and the effects of basic environmental parameters on, a microelectromechanical (MEMS) hydrogen sensor. The sensor contains an array of 10 micromachined cantilever beams. Each cantilever is 500 mum wide x 267 mum long x 2 mum thick and has a capacitance readout capable of measuring cantilever deflection to within 1 nm. A 20-nm-thick coating of 90% palladium-10% nickel bends some of the cantilevers in the presence of hydrogen. The palladium-nickel coatings are deposited in ultra-high-vacuum (UHV) to ensure freedom from a "relaxation" artifact apparently caused by oxidation of the coatings. The sensor consumes 84 mW of power in continuous operation, and can detect hydrogen concentrations between 0.1 and 100% with a roughly linear response between 10 and 90% hydrogen. The response magnitude decreases with increasing temperature, humidity, and oxygen concentration, and the response time decreases with increasing temperature and hydrogen concentration. The 0-90% response time of an unheated cantilever to 1% hydrogen in air is about 90 s at 25 degreesC and 0% humidity. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:120 / 131
页数:12
相关论文
共 24 条
[1]   A chemical sensor based on a microfabricated cantilever array with simultaneous resonance-frequency and bending readout [J].
Battiston, FM ;
Ramseyer, JP ;
Lang, HP ;
Baller, MK ;
Gerber, C ;
Gimzewski, JK ;
Meyer, E ;
Güntherodt, HJ .
SENSORS AND ACTUATORS B-CHEMICAL, 2001, 77 (1-2) :122-131
[2]   Multiple-input microcantilever sensors [J].
Britton, CL ;
Jones, RL ;
Oden, PI ;
Hu, Z ;
Warmack, RJ ;
Smith, SF ;
Bryan, WL ;
Rochelle, JM .
ULTRAMICROSCOPY, 2000, 82 (1-4) :17-21
[3]   KINETICS OF THE MICROMIRROR CHEMICAL SENSOR [J].
BUTLER, MA ;
BUSS, RJ .
SENSORS AND ACTUATORS B-CHEMICAL, 1993, 11 (1-3) :161-166
[4]   HYDROGEN SENSING WITH PALLADIUM-COATED OPTICAL FIBERS [J].
BUTLER, MA ;
GINLEY, DS .
JOURNAL OF APPLIED PHYSICS, 1988, 64 (07) :3706-3712
[5]   Translating biomolecular recognition into nanomechanics [J].
Fritz, J ;
Baller, MK ;
Lang, HP ;
Rothuizen, H ;
Vettiger, P ;
Meyer, E ;
Güntherodt, HJ ;
Gerber, C ;
Gimzewski, JK .
SCIENCE, 2000, 288 (5464) :316-318
[6]  
GLASS RS, 2000, SENSOR NEEDS REQUIRE
[7]  
Glassman I., 1996, COMBUSTION, P589
[8]   Cantilever-based optical deflection assay for discrimination of DNA single-nucleotide mismatches [J].
Hansen, KM ;
Ji, HF ;
Wu, GH ;
Datar, R ;
Cote, R ;
Majumdar, A ;
Thundat, T .
ANALYTICAL CHEMISTRY, 2001, 73 (07) :1567-1571
[9]  
HOFFHEINS BS, 1994, P SOC PHOTO-OPT INS, V2369, P542
[10]  
HUNTER GW, 1992, 105878 NASA