Fabrication of ordered flower-like ZnO nanostructures by a microwave and ultrasonic combined technique and their enhanced photocatalytic activity

被引:57
作者
Li, Hui [1 ,2 ]
Liu, Er-tao [1 ,2 ]
Chan, Frankie Y. F. [3 ]
Lu, Zhong [1 ,2 ]
Chen, Rong [1 ,2 ]
机构
[1] Wuhan Inst Technol, Key Lab Green Chem Proc, Minist Educ, Wuhan 430073, Peoples R China
[2] Wuhan Inst Technol, Sch Chem Engn & Pharm, Wuhan 430073, Peoples R China
[3] Univ Hong Kong, Electron Microscope Unit, Hong Kong, Hong Kong, Peoples R China
关键词
Nanocrystalline materials; Microstructure; ZnO; Flower-like; Microwave; Ultrasonic; FACILE SYNTHESIS; DIRECT GROWTH; ARRAYS;
D O I
10.1016/j.matlet.2011.07.049
中图分类号
T [工业技术];
学科分类号
120111 [工业工程];
摘要
Ordered flower-like zinc oxide (ZnO) nanostructures were fabricated via a facile microwave and ultrasonic combined technique. The product was characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and selected area electron diffraction pattern (SAED). The flower-like ZnO nanostructures were assembled by a central petal and six symmetrical petals which grew radially from the center. The flower-like ZnO sample showed an enhanced photocatalytic performance compared with the ZnO microrods for the methylene blue (MB) degradation, which could be attributed to its special structure feature. Au/ZnO and Ag/ZnO nanocomposites were also synthesized and exhibited enhanced photocatalytic efficiency after decorating noble metal nanoparticles on the surface of flower-like ZnO nanostructures. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:3440 / 3443
页数:4
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