In-Depth Characterization of Prebiotic Galacto-oligosaccharides by a Combination of Analytical Techniques

被引:98
作者
Coulier, Leon [1 ]
Timmermans, Johan [1 ]
Bas, Richard [1 ]
Van Den Dool, Ron [1 ]
Haaksman, Ingrid [1 ]
Klarenbeck, Bert [2 ]
Slaghek, Ted [1 ]
Van Dongen, William [1 ]
机构
[1] TNO Qual Life, NL-3704 HE Zeist, Netherlands
[2] FrieslandCampina Domo, NL-8017 JD Zwolle, Netherlands
关键词
Galacto-oligosaccharides; prebiotics; identification; quantification; high-performance anion-exchange chromatography; mass spectrometry; NMR; HILIC; GC-MS; analysis; ANION-EXCHANGE CHROMATOGRAPHY; BETA-GALACTOSIDASE; LACTOSE HYDROLYSIS; MASS-SPECTROMETRY; KLUYVEROMYCES-LACTIS; ENZYMATIC LACTOSE; TRANSGALACTOSYLATION; TRISACCHARIDES; SPECTROSCOPY; LACTULOSE;
D O I
10.1021/jf902549e
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
A commercial prebiotic galacto-oligosaccharide mixture (Vivinal GOS) was extensively characterized (DP) to the identify and concentration of individual (HPAEC) to (MS) was determined to be especially suitable to assign the DP of individual m/z values as well as their quantification using external (SEC) and hydrophilic interaction liquid chromatography (HILIC) was
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收藏
页码:8488 / 8495
页数:8
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