On Scale Up of Organic Reactions in Closed Vessel Microwave Systems

被引:46
作者
Strauss, Christopher R. [1 ,2 ]
机构
[1] Queens Univ Belfast, QUILL Ctr, Belfast BT9 5AG, Antrim, North Ireland
[2] Strauss Consulting Ltd, Kunyung LPO, Mt Eliza, Vic 3930, Australia
关键词
ASSISTED SYNTHESIS; CHEMICAL-REACTIONS; ENERGY EFFICIENCY; HEATING ELEMENTS; IONIC LIQUID; FLOW; CHEMISTRY; GREEN; BATCH; REACTOR;
D O I
10.1021/op900194z
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Scale up of reactions with existing laboratory-scale microwave technologies and factors affecting extension of the scope, including the influences of putative nonthermal microwave "effects," mechanisms of energy transfer, interactions of microwaves with materials, temperature measurement, and reproducibility between systems, are discussed.
引用
收藏
页码:915 / 923
页数:9
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