High-performance liquid chromatographic determination of Maillard compounds in store-brand and name-brand ultra-high-temperature-treated cows' milk

被引:60
作者
Ferrer, E [1 ]
Alegría, A [1 ]
Courtois, G [1 ]
Farré, R [1 ]
机构
[1] Univ Valencia, Fac Pharm, E-46100 Burjassot, Spain
关键词
milk; food analysis; furosine; furfurals;
D O I
10.1016/S0021-9673(00)00218-1
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Furosine and furfural products of the Maillard reaction are used as specific indicators of the effect of heating treatments on milk quality. Their contents were measured in representative, samples of store- and name-brand ultra-high-temperature-treated milks using RP-HPLC with UV detection. Furosine contents ranged from 40.32 to 50.67 and from 65.48 to 310.58 mg/100 g protein in name- and store-brand milks, respectively. Of the furfurals, only hydroxymethylfurfural was detected. The free hydroxymethylfurfural contents of store-brand milks ranged from 0.22 to 1.70 mg/100 g protein. Total hydroxymethylfurfural contents ranged from 0.29 to 0.41 and from 0.72 to 2.21 mg/100 g protein, for name- and store-brands, respectively. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:599 / 606
页数:8
相关论文
共 33 条
[1]   Changes in furfural compounds during storage of infant milks [J].
Albalá-Hurtado, S ;
Veciana-Nogués, MT ;
Mariné-Font, A ;
Vidal-Carou, MC .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1998, 46 (08) :2998-3003
[2]   Determination of free and total furfural compounds in infant milk formulas by high-performance liquid chromatography [J].
AlbalaHurtado, S ;
VecianaNogues, MT ;
IzquierdoPulido, M ;
VidalCarou, MC .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (06) :2128-2133
[3]  
[Anonymous], 1990, ITAL J FOOD SCI
[4]  
*AOAC, 1980, OFF METH AN, P807
[5]   MAILLARD BROWNING KINETICS IN A LIQUID MODEL SYSTEM [J].
BAISIER, WM ;
LABUZA, TP .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1992, 40 (05) :707-713
[6]   DETERMINATION OF FUROSINE BY GAS-LIQUID CHROMATOGRAPHY [J].
BUSER, W ;
ERBERSDOBLER, HF .
JOURNAL OF CHROMATOGRAPHY, 1985, 346 (OCT) :363-368
[7]   CHANGES IN FUROSINE AND PROTEINS OF UHT-TREATED MILKS STORED AT HIGH AMBIENT-TEMPERATURES [J].
CORZO, N ;
LOPEZFANDINO, R ;
DELGADO, T ;
RAMOS, M ;
OLANO, A .
ZEITSCHRIFT FUR LEBENSMITTEL-UNTERSUCHUNG UND-FORSCHUNG, 1994, 198 (04) :302-306
[8]   RATIO OF LACTULOSE TO FUROSINE AS INDICATOR OF QUALITY OF COMMERCIAL MILKS [J].
CORZO, N ;
DELGADO, T ;
TROYANO, E ;
OLANO, A .
JOURNAL OF FOOD PROTECTION, 1994, 57 (08) :737-739
[9]  
CORZO N, 1991, ALIMENTACION EQUIPOS, V6, P73
[10]   DETERMINATION OF FUROSINE IN MILK SAMPLES BY ION-PAIR REVERSED PHASE LIQUID-CHROMATOGRAPHY [J].
DELGADO, T ;
CORZO, N ;
SANTAMARIA, G ;
JIMENO, ML ;
OLANO, A .
CHROMATOGRAPHIA, 1992, 33 (7-8) :374-376