Synthesis of single crystalline hematite polyhedral nanorods via a facile hydrothermal process

被引：21

作者：

Jia, Baoping ^{[1
]}

Gao, Lian ^{[1
]}

Sun, Jing ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2007年 / 90卷 / 04期

关键词：

D O I：

10.1111/j.1551-2916.2007.01523.x

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Single-crystalline alpha-Fe2O3 nanorods with a polyhedral configuration have been successfully synthesized via a facile hydrothermal process at 180 degrees C. X-ray powder diffraction, transmission electron microscopy observations, field emission scanning electron microscopy, and selected area electron diffraction patterns were used to characterize the as-synthesized samples. The result reveals that goethite nanorods were first generated and then transformed into hematite via dehydration in the successive hydrothermal treatment, in which the alpha-Fe2O3 inherited the rod-like morphology of the goethite precursor. The effect of surfactant and treatment time on the phase and morphology of the final products has been studied, and a possible growth mechanism is proposed.

引用

页码：1315 / 1318

页数：4

共 35 条

[31] Thermally stable hematite hollow nanowires [J].