Real time observation of microwave-enhanced reactions via fast FTIR spectroscopy

被引：8

作者：

Heller, Eberhard ^{[1
]}

Lautenschlaeger, Werner ^{[2
]}

Holzgrabe, Ulrike ^{[1
]}

机构：

[1] Univ Wurzburg, Inst Pharm & Food Chem, D-97074 Wurzburg, Germany

[2] Mikrowellenlaborsyst GmbH, D-88299 Leutkirch Allgau, Germany

来源：

TETRAHEDRON LETTERS | 2009年 / 50卷 / 12期

关键词：

Microwave-enhanced synthesis; Real time observation; Fast FTIR spectroscopy; PROBE;

D O I：

10.1016/j.tetlet.2009.01.035

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Microwave-enhanced reactions are very fast in comparison to thermal reactions. The determination of optimal end point often fails because conventional analytical methods are too slow. Therefore, we established a fast method using FTIR spectroscopy. The result of the reaction control analysis is obtained within less than 1 min. (C) 2009 Elsevier Ltd. All rights reserved.

引用

页码：1321 / 1323

页数：3

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