Preparation of CdS nanowires by the decomposition of the complex in the presence of microwave irradiation

被引:35
作者
He, J
Zhao, XN
Zhu, JJ [1 ]
Wang, J
机构
[1] Nanjing Univ, Dept Chem, Lab Mesoscop Mat Sci, Nanjing 210093, Peoples R China
[2] Huainan Inst Technol, Dept Chem Engn, Huainan 232001, Peoples R China
基金
中国国家自然科学基金;
关键词
crystal morphology; X-ray diffraction; nanostructures; sulfides; nanomaterials; semiconducting II-VI materials;
D O I
10.1016/S0022-0248(02)00944-2
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
A novel synthetic route for the preparation of US nanowires has been developed. US nanowires with a diameter of ca. 4nm have been successfully prepared by the microwave irradiation of a complex of cadmium-1-pyrrlidine dithio carboxylic acid ammonium (C5H12N2S2, APDTC) [Cd(APDTC)(2)](2) in an ethylenediamine solution. The US nanowires were characterized by powder X-ray diffraction pattern, transmission electron microscopy (TEM), UV-Vis spectroscopy, diffuse reflection spectroscopy and PL spectroscopy. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:389 / 394
页数:6
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