Optimization of Ultrasonic-Assisted Extraction of Active Compounds from the Fruit of Star Anise by Using Response Surface Methodology

被引：11

作者：

Lee, A. Yeong ^{[1
]}

Kim, Hyo Seon ^{[1
]}

Choi, Goya ^{[1
]}

Moon, Byeong Cheol ^{[1
]}

Chun, Jin Mi ^{[1
]}

Kim, Ho Kyoung ^{[1
]}

机构：

[1] Korea Inst Oriental Med, Herbal Med Res Div, Herbal Med Resources Grp, Taejon 305811, South Korea

来源：

FOOD ANALYTICAL METHODS | 2014年 / 7卷 / 08期

关键词：

Star anise; p-Anisaldehyde; Anethole; Optimum extraction condition; Central composite design; Response surface methodology; ILLICIUM-VERUM; ANETHOLE; OIL;

D O I：

10.1007/s12161-014-9803-0

中图分类号：

TS2 [食品工业];

学科分类号：

100403 [营养与食品卫生学];

摘要：

p-Anisaldehyde and anethole, the main constituents of the fruit of star anise (Illicium verum Hook.f.), were analyzed by ultra-high-performance liquid chromatography with a diode array detector. The optimum extraction conditions for the two components were determined with response surface methodology, and the experimental factors were planned using central composite design. The adequacy model of this experimental design for p-anisaldehyde and anethole was verified by analysis of variance, and the adjusted regression coefficients (R (2)) were calculated as 0.837 and 0.884, respectively. The p values of lack of fit for p-anisaldehyde and anethole were determined as 0.777 and 0.657, respectively. The maximum yields of the two compounds were predicted to be 0.402 and 7.996 % when the extraction was carried out at 63 A degrees C for 15 min in 81 % ethanol. In the same condition, actual maximum yields of p-anisaldehyde and anethole were 0.422 (+/- 0.008) and 8.017 % (+/- 0.119), respectively.

引用

页码：1661 / 1670

页数：10

共 24 条

[1]

Production and optimization of carotenoid-enriched dried distiller's grains with solubles by Phaffia rhodozyma and Sporobolomyces roseus fermentation of whole stillage [J].