Synthesis and characterisation of zinc oxide tetrapod nanocrystals

被引:43
作者
Newton, Marcus C. [1 ]
Firth, Steven [1 ]
Matsuura, Takashi [1 ]
Warburton, Paul A. [1 ]
机构
[1] UCL, Dept Elect & Elect Engn, Torrington Pl, London WC1E 7JE, England
来源
EMAG-NANO 2005: IMAGING, ANALYSIS AND FABRICATION ON THE NANOSCALE | 2006年 / 26卷
关键词
D O I
10.1088/1742-6596/26/1/060
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Zinc oxide is an important group II-VI semiconductor material with optical properties that permit stable- emission at room temperature. We report on the synthesis of highly uniform nanocrystalline ZnO tetrapod (ZnO-T) nanostructures through a modified chemical vapour transport process. These self assembled nanocrystals are characterised by four cylindrical arms with a hexagonal facet all of which are joined at a tetrahedral core. Studies are carried out on ZnO tetrapods using scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), photoluminescence spectroscopy (PLS) and Raman measurements. We find a simple technique to quench visible emission found in ZnO tetrapods as grown. We also observe Raman active modes suggesting that nitrogen is incorporated within our samples.
引用
收藏
页码:251 / +
页数:2
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