Determination of selenium in infant foods using electrothermal atomic absorption spectrometry with direct slurry sample introduction

被引:8
作者
Baralkiewicz, D
El-Sayed, U
Filipiak, M
Gramowska, H
Mleczek, M
机构
[1] Adam Mickiewicz Univ Poznan, Fac Chem, PL-60613 Poznan, Poland
[2] Poznan Univ Econ, Chair Biochem & Microbiol, PL-60967 Poznan, Poland
来源
CENTRAL EUROPEAN JOURNAL OF CHEMISTRY | 2004年 / 2卷 / 02期
关键词
selenium; infant foods; slurry sampling atomic absorption spectrometry (SS ETAAS);
D O I
10.2478/BF02475577
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Slurry sampling electrothermal atomic absorption (SS ETAAS) was applied to the development of a sensitive and precise method for selenium determination in infant foods without sample pretreatment. Suspensions prepared in a medium containing 0.1% Triton X-100, 0.5 or 5% v/v concentrated HNO3 were directly introduced into the furnace. The accuracy of the procedure was confirmed by analysis of a standard reference material and comparison with hydride generation atomic absorption spectrometric (HGAAS) procedure. The characteristic mass is 44 pg and detection limit 0.43 mug.l(-1). (C) Central European Science Journals. All rights reserved.
引用
收藏
页码:334 / 346
页数:13
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