Process intensification: Precipitation of barium sulfate using a spinning disk reactor

被引:92
作者
Cafiero, LM
Baffi, G
Chianese, A
Jachuck, RJJ
机构
[1] Univ Roma La Sapienza, Dept Chem Engn, I-00184 Rome, Italy
[2] Univ Newcastle Upon Tyne, Proc Intensificat & Innovat Ctr, Dept Chem & Proc Engn, PIIC, Newcastle Upon Tyne NE1 7RU, Tyne & Wear, England
关键词
D O I
10.1021/ie010654w
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
In this work, the use of a spinning disk reactor as a unit for a reaction-precipitation process is investigated. An experimental study is reported concerning the precipitation of barium sulfate from aqueous solutions at 25 degreesC on a spinning disk of 0.5 m in diameter. At a rotational speed higher than 900 rpm, spontaneous precipitation took place and crystals similar to0.7 mum in size were produced. At a supersaturation ratio of 2000, the number of generated crystals is comparable with those reported in the literature when a T-mixer is used, but in the case of the spinning disk, a much lower specific dispersed power is required.
引用
收藏
页码:5240 / 5246
页数:7
相关论文
共 13 条
[1]  
BENET N, 1999, 14 INT S IND CRYST C
[2]   Process intensification: spinning disk reactor for styrene polymerisation [J].
Boodhoo, KVK ;
Jachuck, RJ .
APPLIED THERMAL ENGINEERING, 2000, 20 (12) :1127-1146
[3]   A STOPPED-FLOW TECHNIQUE IN FAST PRECIPITATION KINETICS - THE CASE OF BARIUM-SULFATE [J].
CAROSSO, PA ;
PELIZZETTI, E .
JOURNAL OF CRYSTAL GROWTH, 1984, 68 (02) :532-536
[4]   MACROMIXING AND MICROMIXING IN STIRRED TANKS [J].
GEISLER, R ;
MERSMANN, A ;
VOIT, H .
CHEMIE INGENIEUR TECHNIK, 1988, 60 (12) :947-955
[5]  
Gluck B., 1988, HYDRODYNAMISCHE GASD
[6]  
HEYER C, 1999, 14 INT S IND CRYST C
[7]   PROCESS INTENSIFICATION - HEAT-TRANSFER CHARACTERISTICS OF TAILORED ROTATING SURFACES [J].
JACHUCK, RJJ ;
RAMSHAW, C .
HEAT RECOVERY SYSTEMS & CHP, 1994, 14 (05) :475-491
[8]  
KIND M, 1999, 14 INT S IND CRYST C
[9]   CHARACTERIZING THE PRODUCT CRYSTALS FROM A MIXING TEE PROCESS [J].
MOHANTY, R ;
BHANDARKAR, S ;
ZUROMSKI, B ;
BROWN, R ;
ESTRIN, J .
AICHE JOURNAL, 1988, 34 (12) :2063-2068
[10]  
MOORE SR, 1996, THESIS U NEWCASTLE T