Synthesis and characterisation of La1-xSrxCoO3 with large surface area

被引:57
作者
Berger, D
Fruth, V
Jitaru, I
Schoonman, J
机构
[1] Politeh Univ Bucharest, Dept Inorgan Chem, Bucharest 78126, Romania
[2] Delft Univ Technol, Inorgan Chem Lab, NL-2628 BL Delft, Netherlands
[3] Acad Romana, Inst Phys Chem, Bucharest 77208, Romania
关键词
perovskites; complex precursor; La(1-x)SrxCoO(3); nanomaterials; high surface area; powder technology;
D O I
10.1016/j.matlet.2004.02.035
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The paper presents a simple technique for synthesis of La1-xSrxCoO3 (v=0-0.3) nanopowders by calcining maleate-based precursors. The complex precursors were characterised by chemical analysis, electronic and FT-IR spectra and DTA-TG analysis. The XRD data for La1-xSrxCoO3 show that the samples are single phase with rhombohedral distorted perovskite structure. Specific surface area results of La1-xSrxCoO3 samples indicated values in the range 30-38 m(2)/g, which are high values for perovskite-type oxides. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:2418 / 2422
页数:5
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