5-[N-(1H-benzotriazol-1-ylmethyl)-amino]-3-tert-butyl-1-phenylpyrazole:: sheets built from N-H •••N, C-H •••N and C-H •••π(pyrazole) interactions

被引：3

作者：

Glidewell, C ^{[1
]}

Low, JN

Cobo, J

Nogueras, M

Sánchez, A

Rengifo, E

Abonia, R

机构：

[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

[2] Univ Aberdeen, Dept Chem, Odl Aberdeen AB24 3UE, Scotland

[3] Univ Jaen, Dept Quim Inorgan & Organ, Jaen 23071, Spain

[4] Univ Valle, Dept Quim, Grp Invest Compuestos Heterocicl, Cali AA25360, Colombia

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2002年 / 58卷 / 06期

关键词：

D O I：

10.1107/S0108270102006881

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In the title compound, C20H22N6, the molecules are linked into a chain of rings by N-H⋯N [H⋯N 2.16 Å, N⋯N 2.950 (3) Å and N-H⋯N 149°] and C-H⋯N [H⋯N 2.55 Å, C⋯N 3.481 (3) Å and C-H⋯N 165°] hydrogen bonds, and these chains are linked into sheets by means of C-H⋯π(pyrazole) interactions.

引用

页码：O314 / O317

页数：4

共 16 条

[1] Synthesis of novel 1,2,5,6-tetrahydro-4H-pyrrolo [3,2,1-ij]-quinolines via benzotriazole methodology [J].

Abonia, R ;

Albornoz, A ;

Insuasty, B ;

Quiroga, J ;

Meier, H ;

Hormaza, A ;

Nogueras, M ;

Sánchez, A ;

Cobo, J ;

Low, JN .

TETRAHEDRON, 2001, 57 (23) :4933-4938

[2]

ABONIA R, 2002, IN PRESS J CHEM S P1

[3]

ALLEN FH, 1993, CHEM DESIGN AUTOMATI, V8, P1

[4] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS [J].

BERNSTEIN, J ;

DAVIS, RE ;

SHIMONI, L ;

CHANG, NL .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) :1555-1573

[5]

*BRUK AXS INC, 1997, SADABS SMART SHELXTL

[6] PROOF OF STRUCTURES DERIVED FROM THE HYDROXY-METHYLATION AND AMINO-METHYLATION OF BENZOTRIAZOLE [J].

BURCKHALTER, JH ;

STEPHENS, VC ;

HALL, LAR .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1952, 74 (15) :3868-3870

[7]

DESIRAJU GR, 1999, WEAK HYDROGEN BOND S, P122

[8]

FERGUSON G, 1999, PRPKAPPA

[9]

GRANDBERG II, 1961, ZH OBSHCH KHIM+, V31, P2311

[10]

Katritzky AR, 1998, SYNTHESIS-STUTTGART, P1487

← 1 2 →