Efficient synthetic method for β-enamino esters using ultrasound

被引：78

作者：

Brandt, CA

da Silva, ACMP

Pancote, CG

Brito, CL

da Silveira, MAB

机构：

[1] Inst Butantan, BR-05503900 Sao Paulo, Brazil

[2] Univ Sao Paulo, Dept Farm, Sao Paulo, Brazil

来源：

SYNTHESIS-STUTTGART | 2004年 / 10期

关键词：

ultrasound; beta-enamino esters; beta-keto esters; amines;

D O I：

10.1055/s-2004-829102

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

beta-Keto esters react with a variety of amines in the presence of 0.1 equivalents of acetic acid without any solvents under ultrasound to give good yields of the corresponding beta-enamino esters.

引用

页码：1557 / 1559

页数：3

共 46 条

[1] REACTIONS OF ENAMINES .V. ACYLATION OF ENAMINO KETONES [J].

ALT, GH ;

SPEZIALE, AJ .

JOURNAL OF ORGANIC CHEMISTRY, 1964, 29 (04) :798-&

[2] Photorearrangement of N-alkanoyl beta-enaminones. Application to the synthesis of alpha-amino-beta,gamma-unsaturated acid derivatives [J].

Amougay, A ;

Letsch, O ;

Pete, JP ;

Piva, O .

TETRAHEDRON, 1996, 52 (07) :2405-2420

[3] The fluoroquinolone antibacterials: past, present and future perspectives [J].

Appelbaum, PC ;

Hunter, PA .

INTERNATIONAL JOURNAL OF ANTIMICROBIAL AGENTS, 2000, 16 (01) :5-15

[4] Gold catalysis in the reactions of 1,3-dicarbonyls with nucleophiles [J].

Arcadi, A ;

Bianchi, G ;

Di Giuseppe, S ;

Marinelli, F .

GREEN CHEMISTRY, 2003, 5 (01) :64-67

[5]

Arend M, 1998, ANGEW CHEM INT EDIT, V37, P1044, DOI 10.1002/(SICI)1521-3773(19980504)37:8<1044::AID-ANIE1044>3.0.CO

[6]

2-E

[7] USE OF BORON-TRIFLUORIDE ETHERATE IN THE PREPARATION OF 2-AMINO-1-ALKENYL KETONES FROM BETA-DIKETONES AND LOW-BOILING AMINES [J].

AZZARO, M ;

GERIBALDI, S ;

VIDEAU, B .

SYNTHESIS-STUTTGART, 1981, (11) :880-881

[8]

BARALDI PG, 1993, SYNTHESIS-STUTTGART, P1206

[9]

BARALDI PG, 1983, SYNTHESIS-STUTTGART, P902

[10] CHEMOSELECTIVE AND DIASTEREOSELECTIVE REDUCTION OF BETA-ENAMINO ESTERS - A CONVENIENT SYNTHESIS OF BOTH CIS-GAMMA-AMINO AND TRANS-GAMMA-AMINO ALCOHOLS AND BETA-AMINO ESTERS [J].

BARTOLI, G ;

CIMARELLI, C ;

MARCANTONI, E ;

PALMIERI, G ;

PETRINI, M .

JOURNAL OF ORGANIC CHEMISTRY, 1994, 59 (18) :5328-5335

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