Synthesis of niobia nanocrystals with controlled morphology

被引：51

作者：

Leite, Edson R. ^{[1
]}

Vila, Cristiane

Bettini, Jefferson

Longo, Elson

机构：

[1] Univ Fed Sao Carlos, Dept Chem, BR-13565905 Sao Carlos, SP, Brazil

[2] Natl Lab Synchrotron Light, Campinas, SP, Brazil

来源：

JOURNAL OF PHYSICAL CHEMISTRY B | 2006年 / 110卷 / 37期

关键词：

D O I：

10.1021/jp0642544

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

In this work, TT niobia-phase nanocrystals with controlled morphology were obtained by the hydrothermal treatment of a niobium peroxo complex precursor at very low temperatures. The materials obtained by this route presented a very high surface area (ranging from 79 to 327 m(2)/g), disordered NbO6, NbO7, and NbO8 polyhedra, Nb-O superficial sites, and a superficial OH group, which must have ensured the acidic characteristics of this oxide.

引用

页码：18088 / 18090

页数：3

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