Microwave-polyol process for Pt and Ag nanoparticles

被引：309

作者：

Komarneni, S ^{[1
]}

Li, DS

Newalkar, B

Katsuki, H

Bhalla, AS

机构：

[1] Penn State Univ, Mat Res Lab, Mat Res Inst, University Pk, PA 16802 USA

[2] SCRL, Saga 8440024, Japan

来源：

LANGMUIR | 2002年 / 18卷 / 15期

关键词：

D O I：

10.1021/la025741n

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The nanophase metal powders such as platinum and silver were prepared using microwave-polyol process. This experiment for the synthesis of nanophase platinum and silver metals were conducted using chloroplanitic acid and silver nitrate as starting precursors. Some of the advantages of the microwave-assisted reactions are selective formation of one phase over another, initial rapid heating which leads to energy savings.

引用

页码：5959 / 5962

页数：4

共 36 条

[11] Chu P., 1988, U.S. Patent, Patent No. [4778666, 4,778,666.]
[12] Dormann JL, 1997, ADV CHEM PHYS, V98, P283, DOI 10.1002/9780470141571.ch4
[13] Fievet F., 1989, M RS Bulletin, V74, P29, DOI [10.1557/S0883769400060930, DOI 10.1557/S0883769400060930]
[14] FIGLARZ M, 1982, Patent No. 8221483
[15] THE USE OF MICROWAVE-OVENS FOR RAPID ORGANIC-SYNTHESIS
GEDYE, R
SMITH, F
WESTAWAY, K
ALI, H
BALDISERA, L
LABERGE, L
ROUSELL, J
[J]. TETRAHEDRON LETTERS, 1986, 27 (03) : 279 - 282
[16] APPLICATION OF COMMERCIAL MICROWAVE-OVENS TO ORGANIC-SYNTHESIS
GIGUERE, RJ
BRAY, TL
DUNCAN, SM
MAJETICH, G
[J]. TETRAHEDRON LETTERS, 1986, 27 (41) : 4945 - 4948
[17] LARGE COAPO-5 SINGLE-CRYSTALS - MICROWAVE SYNTHESIS AND ANISOTROPIC OPTICAL-ABSORPTION
GIRNUS, I
HOFFMANN, K
MARLOW, F
CARO, J
DORING, G
[J]. MICROPOROUS MATERIALS, 1994, 2 (06): : 537 - 541
[18] LARGE ALPO4-5 CRYSTALS BY MICROWAVE-HEATING
GIRNUS, I
JANCKE, K
VETTER, R
RICHTERMENDAU, J
CARO, J
[J]. ZEOLITES, 1995, 15 (01): : 33 - 39
[19] APPLICATION OF MICROWAVE DIELECTRIC LOSS HEATING EFFECTS FOR THE RAPID AND CONVENIENT SYNTHESIS OF RUTHENIUM(II) POLYPYRIDINE COMPLEXES
GREENE, DL
MINGOS, DMP
[J]. TRANSITION METAL CHEMISTRY, 1991, 16 (01) : 71 - 72
[20] Jansen J. C., 1992, SYNTHESIS MICROPOROU, V1, P507

← 1 2 3 4 →