A practical method for the analysis of overlapped peaks in energy dispersive X-ray spectra

被引:43
作者
Sahin, Y
Karabulut, A
Budak, G
机构
[1] Atatürk University, Faculty of Arts and Sciencies, Department of Physics
关键词
D O I
10.1080/05704929608000573
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
In this study a practical method for the spectral analysis of some overlapped characteristic X-ray peaks is presented. The overlapped characteristic K-alpha and K-beta peaks and the artificially overlapped two K-alpha peaks (peak doublet) of arsenic obtained by the radioisotope-excited, energy dispersive X-ray fluorescence (EDXRF) technique, are resolved. A total of 34 overlapped peak systems were investigated: the proposed method provided 18 reliable results, whereas the first and the second methods gave 15 and 1, respectively. The intensity ratios of K-beta/K-alpha obtained by the novel method are also in good agreement with the theoretical relativistic Hartree-Slater values.
引用
收藏
页码:333 / 345
页数:13
相关论文
共 16 条
[1]  
Bertin E.P., 1975, Principles and Practice of X-ray Spectrometric Analysis
[2]   IMPROVED MODEL FOR THE INTENSITY OF LOW-ENERGY TAILING IN SI(LI) X-RAY-SPECTRA [J].
CAMPBELL, JL ;
WANG, JX .
X-RAY SPECTROMETRY, 1991, 20 (04) :191-197
[3]  
DELBROUCKHABARU JM, 1984, NUCL INSTRUM METH B, V3, P316
[4]  
DOJO M, 1974, NUCL INSTRUM METHODS, V115, P426
[5]   LEVEL STRUCTURE OF TM-171 [J].
GRAHAM, RL ;
GEIGER, JS ;
JOHNS, MW .
CANADIAN JOURNAL OF PHYSICS, 1972, 50 (06) :513-&
[6]   ANALYTICAL FUNCTIONS FOR FITTING PEAKS FROM GE SEMICONDUCTOR-DETECTORS [J].
HELMER, RG ;
LEE, MA .
NUCLEAR INSTRUMENTS & METHODS, 1980, 178 (2-3) :499-512
[7]   DETERMINATION OF PEAK AREA [J].
KOKTA, L .
NUCLEAR INSTRUMENTS & METHODS, 1973, 112 (1-2) :245-251
[8]   CHEMICAL EFFECTS ON K-BETA/K-BETA X-RAY-INTENSITY RATIOS IN COORDINATION-COMPOUNDS OF SOME 3D ELEMENTS [J].
KUCUKONDER, A ;
SAHIN, Y ;
BUYUKKASAP, E ;
KOPYA, A .
JOURNAL OF PHYSICS B-ATOMIC MOLECULAR AND OPTICAL PHYSICS, 1993, 26 (01) :101-105
[9]   NEW METHOD FOR REPRESENTATION OF PEAK DETECTION - GE(LI) [J].
LIBERT, J .
NUCLEAR INSTRUMENTS & METHODS, 1973, 109 (03) :609-611
[10]   PEAK AREA DETERMINATION FOR GE(LI) DETECTOR DATA [J].
QUITTNER, P .
NUCLEAR INSTRUMENTS & METHODS, 1969, 76 (01) :115-&