A novel proton-transfer compound: piperazinium oxalate monohydrate

被引:12
作者
Aghabozorg, Hossein
Ghadermazi, Mohammad
Sheshmani, Shabnam
机构
[1] Teacher Training Univ, Dept Chem, Tehran 15614, Iran
[2] Islamic Azad Univ, Dept Chem, Shahr E Rey Branch, Tehran, Iran
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷
关键词
CRYSTAL-STRUCTURE; 2,6-PYRIDINEDICARBOXYLIC ACID; DIPICOLINIC ACID; X-RAY; COMPLEX;
D O I
10.1107/S1600536806025359
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The asymmetric unit of the title compound, C4H12N22+center dot C2O42-center dot H2O, contains one water molecule, one anion and two half-cations, both cations having chair conformations. The crystal structure is stabilized by intra- and intermolecular O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds, linking the molecules into a three-dimensional framework, which results in the formation of a supramolecular structure based on a hydrogen-bonded network.
引用
收藏
页码:O3287 / O3289
页数:3
相关论文
共 16 条
[1]   Novel complexes of gallium(III), indium(III), and thallium(III) with pyridine-containing proton transfer ion pairs obtained from dipicolinic acid - Synthesis, characterization and X-ray crystal structure [J].
Aghabozorg, H ;
Ramezanipour, F ;
Kheirollahi, PD ;
Saei, AA ;
Shokrollahi, A ;
Shamsipur, M ;
Manteghi, F ;
Soleimannejad, J ;
Sharif, MA .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2006, 632 (01) :147-154
[2]   2,6-Diaminopyridinium pyridinium-2,6-dicarboxylate: a redetermination [J].
Aghabozorg, H ;
Saei, AA ;
Ramezanipour, F .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O3242-O3244
[3]  
AGHABOZORG H, 2005, ANAL SCI, V261, pX73
[4]   Bis(propane-1,3-diaminium) tris(pyridine-2,6-dicarboxylato-κ3O,N,O′)cerate(III) nitrate 3.5-hydrate [J].
Aghabozorg, Hossein ;
Nakhjavan, Bahar ;
Ghadermazi, Mohammad ;
Ramezanipour, Farshid .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 :M1527-M1529
[5]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[6]  
[Anonymous], 1998, SADABS VERSION 2 01
[7]  
BRUKER, 1998, SAINT PLUS VERSION 6
[8]  
BRUKER, 2000, GEMINI VERSION 1 02
[9]   GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].
CREMER, D ;
POPLE, JA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358
[10]   First anionic 1,10-phenanthroline-2,9-dicarboxylate containing metal complex obtained from a novel 1:1 proton-transfer compound:: Synthesis, characterization, crystal structure, and solution studies [J].
Moghimi, A ;
Alizadeh, R ;
Shokrollahi, A ;
Aghabozorg, H ;
Shamsipur, M ;
Shockravi, A .
INORGANIC CHEMISTRY, 2003, 42 (05) :1616-1624