Direct preparation of cyclodextrin monophosphates

被引：13

作者：

Tarelli, E ^{[1
]}

Lemercinier, X ^{[1
]}

Wheeler, S ^{[1
]}

机构：

[1] NATL INST BIOL STAND & CONTROLS, POTTERS BAR EN6 3QG, HERTS, ENGLAND

来源：

CARBOHYDRATE RESEARCH | 1997年 / 302卷 / 1-2期

关键词：

cyclodextrins; phosphate; esters; metaphosphate; direct preparation;

D O I：

10.1016/S0008-6215(97)00108-0

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Aqueous solutions of cyclodextrins and inorganic metaphosphate at pH 4, upon drying and subsequent warming, produce mixtures of isomeric monophosphate esters which are amenable to separation by anion-exchange chromatography. The products are characterised by enzymatic, mass, and NMR spectroscopic analysis. The methodology provides a route to these derivatives by a single reaction. (C) 1997 Elsevier Science Ltd. (C) 1997 Elsevier Science Ltd.

引用

页码：27 / 34

页数：8

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